Hughes, Gregory; Wang, Changsheng; Batsanov, Andrei S.; Fern, Michael; Frank, Stephen; Bryce, Martin R.; Perepichka, Igor F.; Monkman, Andrew P.; Lyons, Benjamin P.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3069 - 3077
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran
T=20°C;
参考文献
Hughes, Gregory; Wang, Changsheng; Batsanov, Andrei S.; Fern, Michael; Frank, Stephen; Bryce, Martin R.; Perepichka, Igor F.; Monkman, Andrew P.; Lyons, Benjamin P.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3069 - 3077
Hughes, Gregory; Wang, Changsheng; Batsanov, Andrei S.; Fern, Michael; Frank, Stephen; Bryce, Martin R.; Perepichka, Igor F.; Monkman, Andrew P.; Lyons, Benjamin P.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3069 - 3077
1: cyanoacetic acid ethyl ester With sodium hydride in tetrahydrofuran
0.166667 h;
2: 2,5-dibromo-pyrimidine in tetrahydrofuran
T=20°C; 6 h;
3: With hydrogenchloride in water
参考文献
BAYER CROPSCIENCE SA
Patent: WO2006/117358 A1, 2006 ;
Location in patent: Page/Page column 37 ;
