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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
32786-26-8
合成路线
（共 10 条）
32786-26-8
+
123-82-0
异庚胺
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
hydrogen; lipase B from Candida antarctica in toluene T=70°C; P=750.075 Torr; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
746564-13-6
反应条件
Candida antarctica lipase B in various solvent(s) T=28°C; 46 h; Further byproducts given;
参考文献
Gonzalez-Sabin, Javier; Gotor, Vicente; Rebolledo, Francisca
Tetrahedron Asymmetry, 2004 , vol. 15, # 3 p. 481 - 488
32786-26-8
+
3319-15-1
4-甲氧基-α-甲基苯甲醇
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1517-70-0
(R)-1-(4-甲氧基苯基)乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
4128-31-8
仲辛醇
+
32786-26-8
→
反应条件
54712-18-4
+
3540-05-4
+
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
+
5391-88-8
1-(4-溴苯基)-1-乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
5391-88-8
1-(4-溴苯基)-1-乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
+
123-82-0
异庚胺
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
hydrogen; lipase B from Candida antarctica in toluene T=70°C; P=750.075 Torr; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
+
5391-88-8
1-(4-溴苯基)-1-乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
5391-88-8
1-(4-溴苯基)-1-乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
+
5391-88-8
1-(4-溴苯基)-1-乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
5391-88-8
1-(4-溴苯基)-1-乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
+
5391-88-8
1-(4-溴苯基)-1-乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
5391-88-8
1-(4-溴苯基)-1-乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
32786-26-8
+
3319-15-1
4-甲氧基-α-甲基苯甲醇
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1517-70-0
(R)-1-(4-甲氧基苯基)乙醇
反应条件
lipase B from Candida antarctica in toluene T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
