3,5-二(三氟甲基)硝基苯合成路线 (共 14 条)
反应条件
sulfuric acid; nitric acid; pyrosulfuric acid
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4967
反应条件
trifluorormethanesulfonic acid; Boron tris(trifluoromethanesulfonate); nitric acid T=20°C; 20 h;
参考文献
Olah, George A.; Orlinkov, Alexander; Oxyzoglou, Alexandros B.; Prakash, G. k. Surya
Journal of Organic Chemistry, 1995 , vol. 60, # 22 p. 7348 - 7350
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Rahaim Jr., Ronald J.; Maleczka Jr., Robert E.
Synthesis, 2006 , # 19 p. 3316 - 3340
反应条件
tetrabutyl ammonium fluoride in acetonitrile T=20°C; 0.0333333 h;
参考文献
Sun, Haoran; DiMagno, Stephen G.
Journal of the American Chemical Society, 2005 , vol. 127, # 7 p. 2050 - 2051
反应条件
1: tin (II)-chloride; aqueous hydrochloric acid / Hydrogenation 2: aqueous hydrochloric acid; sodium nitrite; potassium iodide View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4967
反应条件
potassium hydroxide in N,N-dimethyl-formamide
参考文献
Gitis,S.S.; L'vovich,I.G.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, # 7 p. 2250 - 2254,2262 - 2265
反应条件
hydrogen; platinum(IV) oxide in methanol T=20 - 25°C; P=36.8 Torr;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1031 - 1038
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1194 - 1202
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Synthesis, , # 19 p. 3316 - 3340
反应条件
hydrogen; platinum(IV) oxide in methanol T=20 - 25°C; P=36.8 Torr; 3 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 1031 - 1038
Zhurnal Organicheskoi Khimii, , vol. 16, # 6 p. 1194 - 1202
反应条件
acetic acid; platinum Hydrogenation;
参考文献
Ross et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 4967