2-甲基-3-苯基丁烷-2-醇合成路线 (共 31 条)
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 4 h; Ambient temperature; Mechanism;
参考文献
Gurudutt, K. N.; Ravindranath, B.
Synthesis, 1983 , # 11 p. 888 - 889
反应条件
sodium in diethyl ether
参考文献
Kochi,J.K.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1960 - 1968
反应条件
1: 82 percent / 4-(N,N-dimethylamino)pyridine 2: 40 percent / Li; naphthalene / tetrahydrofuran / 2 h / -30 °C View Scheme
参考文献
Alonso, Emma; Guijarro, David; Martinez, Pedro; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1999 , vol. 55, # 36 p. 11027 - 11038
反应条件
air in acetone 24 h; Ambient temperatureIrradiation; Yield given;
参考文献
Pasternak, Mordechai; Morduchowitz, Abraham
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4275 - 4278
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; tetra-n-butylammonium perchlorate T=0°C; current density = 25 mA/cm2, 2.0 F/mol of halide;
参考文献
Satoh; Suginome; Tokuda
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1791 - 1794
反应条件
perchloric acid in 1,4-dioxane T=100°C; Equilibrium constant;
参考文献
Laurent,A. et al.
Bulletin de la Societe Chimique de France, 1968 , p. 3307 - 3314
反应条件
naphthalene; lithium 1.) THF, -40 deg C, 45 min, 2.) THF, -40 deg C, 1 h, 3.) THF, -40 to 20 deg C, overnight; Yield given. Multistep reaction;
参考文献
Gil, Juan F.; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1993 , vol. 49, # 42 p. 9535 - 9546
反应条件
in acetone 24 h; Ambient temperatureIrradiation; Yield given;
参考文献
Pasternak, Mordechai; Morduchowitz, Abraham
Tetrahedron Letters, 1983 , vol. 24, # 33 p. 3439 - 3442
反应条件
air 24 h; Ambient temperatureIrradiation; Yields of byproduct given;
参考文献
Pasternak, Mordechai; Morduchowitz, Abraham
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4275 - 4278
参考文献
Lepin
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1190
Chem. Zentralbl., 1912 , vol. 83, # II p. 2082