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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯乙酰乙酸甲酯
合成路线
（共 50 条）
32807-28-6
4-氯乙酰乙酸甲酯
→
反应条件
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
nicotinamide adenine dinucleotide; isopropyl alcohol in hexane; water Ambient temperaturePED alcohol dehydrogenase, phosphate buffer pH 7.1;
参考文献
Bradshaw, Curt W.; Fu, Hong; Shen, Gwo-Jenn; Wong, Chi-Huey
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1526 - 1532
4128-31-8
仲辛醇
+
32807-28-6
4-氯乙酰乙酸甲酯
→
反应条件
6169-06-8
(S)-(+)-2-辛醇
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
4630-06-2
6-甲基-5-庚烯-2-醇
+
32807-28-6
4-氯乙酰乙酸甲酯
→
反应条件
58917-26-3
(S)-(+)-6-甲基-5-庚烯-2-醇
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
32807-28-6
4-氯乙酰乙酸甲酯
+
98-85-1
DL-1-苯乙醇
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
32807-28-6
4-氯乙酰乙酸甲酯
+
3319-15-1
4-甲氧基-α-甲基苯甲醇
→
反应条件
1517-70-0
(R)-1-(4-甲氧基苯基)乙醇
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
32807-28-6
4-氯乙酰乙酸甲酯
+
1193-81-3
1-环己基乙醇
→
反应条件
3113-98-2
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
32807-28-6
4-氯乙酰乙酸甲酯
→
反应条件
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
+
88759-59-5
反应条件
sodium azide; alcohol dehydrogenase from Lactobacillus brevis; halohydrin dehalogenase from Mycobacterium sp. GP1; NADPH; isopropyl alcohol T=30°C; pH=7.5; 24 h; aq. bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2293 - 2298
32807-28-6
4-氯乙酰乙酸甲酯
+
120121-01-9
→
反应条件
135145-34-5
+
120121-01-9
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
32807-28-6
4-氯乙酰乙酸甲酯
→
反应条件
127001-17-6
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
+
88246-12-2
反应条件
1: With Lactobacillus brevis alcohol dehydrogenase; isopropyl alcohol T=30°C; 4 h; aq. bufferEnzymatic reaction; 2: With Mycobacterium sp. GP1 halohydrin dehalogenase HheB T=30°C; 20 h; aq. bufferEnzymatic reaction; optical yield given as percent eestereoselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 4 p. 483 - 488
32807-28-6
4-氯乙酰乙酸甲酯
→
反应条件
88496-70-2
+
86728-93-0
(S)-4-氯-3-羟基丁酸甲酯
反应条件
T=30°C; 24 h; Kroekera sp. No. 2201 (AKU 4705) growning in methanol; Yields of byproduct given;
参考文献
Ushio, Kazutoshi; Inouye, Kiyoko; Nakamura, Kaoru; Oka, Shinzaburo; Ohno, Atsuyoshi
Tetrahedron Letters, 1986 , vol. 27, # 23 p. 2657 - 2660
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