2-甲基-5-己烯-3-醇合成路线 （共 20 条）
反应条件
1: With tin T=20°C; Barbier reaction; 24 h; Ionic liquid; 2: With water Ionic liquid;
参考文献
Slaton, Rahiem; Petrone, Adam; Manchanayakage, Renuka
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5073 - 5076
反应条件
[Eu2(fumarate)3(H2O)4]⋅3H2O in dichloromethane; water T=25°C; 0.25 h;
参考文献
Freitas, Juliano C.R.; De Oliveira, Cristiane K.; Cunha, Edilanio C.; Malvestiti, Ivani; Alves Jr., Severino; Longo, Ricardo L.; Menezes, Paulo H.
Tetrahedron Letters, 2013 , vol. 54, # 12 p. 1558 - 1561
反应条件
tin(ll) chloride; Pd(TPPMS)2Cl2 in n-heptane; water T=35°C; 7 h;
参考文献
Okano, Tamon; Kiji, Jitsuo; Doi, Takanori
Chemistry Letters, 1998 , # 1 p. 5 - 6
反应条件
in diethyl ether T=0 - 20°C; 1 h;
参考文献
Zorn, Nicolas; Lett, Robert
Tetrahedron Letters, 2006 , vol. 47, # 26 p. 4325 - 4330
反应条件
zirconium(IV) oxychloride in water T=60°C; 5 h;
参考文献
Shen, Wei; Wang, Li-Min; Feng, Jian-Jun; Tian, He
Tetrahedron Letters, 2008 , vol. 49, # 25 p. 4047 - 4049
反应条件
1: With (IPr)CuF; n-octyltrifluorosilane in tetrahydrofuran T=20°C; 48 h; Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran 1 h; Inert atmosphere;
参考文献
Russo, Vlncenzo; Herron, Jessica R.; Ball, Zachary T.
Organic Letters, 2010 , vol. 12, # 2 p. 220 - 223
反应条件
(R)-4-benzylsulfinylmethyl-2-phenyl-4,5-dihydro-oxazole; N-ethyl-N,N-diisopropylamine in dichloromethane T=-21°C; 48 h;
参考文献
Rowlands, Gareth J.; Barnes, William Kentish
Chemical Communications, 2003 , # 21 p. 2712 - 2713
反应条件
SnF2; 10,11-dihydro-5-[3-(methylamino)propyl]-5H-dibenz(b,f)azepin in N,N-dimethyl-formamide Ambient temperature;
参考文献
Borch, Richard F.; Canute, Gregory W.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 10 p. 3044 - 3052
反应条件
C20H23BBiF4N in methanol; water T=20°C; 1 h;
参考文献
Zhang, Xiaowen; Qiu, Renhua; Tan, Nianyuan; Yin, Shuangfeng; Xia, Jun; Luo, Shenglian; Au, Chak-Tong
Tetrahedron Letters, 2010 , vol. 51, # 1 p. 153 - 156
反应条件
in tetrahydrofuran T=0 - 20°C; 1.25 h;
参考文献
Taillier, Catherine; Hameury, Thomas; Bellosta, Veronique; Cossy, Janine
Tetrahedron, 2007 , vol. 63, # 21 p. 4472 - 4490
