2-甲基-5-己烯-3-醇合成路线 （共 20 条）
反应条件
(i) AlCl3, (ii) aq. MeOH; Multistep reaction;
参考文献
Tetrahedron Letters, , p. 2449 - 2450
反应条件
samarium diiodide in tetrahydrofuran 1.5 h; Ambient temperature;
参考文献
Souppe, J.; Namy, J. L.; Kagan, H. B.
Tetrahedron Letters, 1982 , vol. 23, # 34 p. 3497 - 3500
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Souppe, J.; Danon, L.; Namy, J.L.; Kagan, H.B.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 227 - 236
反应条件
1: Brown asymmetric allylation; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide Brown asymmetric allylation; Inert atmosphere;
参考文献
Cho, Hee Yeon; Morken, James P.
Journal of the American Chemical Society, 2010 , vol. 132, # 22 p. 7576 - 7577
反应条件
perchloric acid; sodium nitrite
参考文献
Journal of Organic Chemistry, , vol. 33, # 10 p. 3841 - 3848
反应条件
in methanol-d4 T=30°C; 192 h; various solvents; Product distribution;
参考文献
Cokley, Teresa M.; Harvey, Peta J.; Marshall, Raymond L.; McCluskey, Adam; Young, David J.
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 1961 - 1964
反应条件
Dehydratisieren nach der Xanthogenatmethode;
参考文献
Karassew; Chabarowa
Zhurnal Obshchei Khimii, 1940 , vol. 10, p. 1645
Chem. Zentralbl., 1942 , vol. 113, # I p. 28
反应条件
Dehydratisieren nach der Xanthogenatmethode;
参考文献
Karassew; Chabarowa
Zhurnal Obshchei Khimii, 1940 , vol. 10, p. 1645
Chem. Zentralbl., 1942 , vol. 113, # I p. 28
反应条件
1: Zn/Cu
2: PCC
View Scheme
参考文献
Bloodworth, A. J.; Korkodilos, Despoina
Tetrahedron Letters, 1991 , vol. 32, # 47 p. 6953 - 6956
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Stokes, Benjamin J.; Opra, Susanne M.; Sigman, Matthew S.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11408 - 11411
反应条件
in Petroleum ether
T=0°C; 12 h;
参考文献
Hoffmann, Reinhard W.; Bewersdorf, Martin
Liebigs Annalen der Chemie, 1992 , # 6 p. 643 - 654
