2-二氮杂-1-苯乙酮合成路线 （共 259 条）
反应条件
boron trifluoride diethyl etherate T=0°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 9 p. 2450 - 2455
反应条件
boron trifluoride diethyl etherate T=0°C;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 9 p. 2450 - 2455
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=80°C; 6 h;
参考文献
Reddy, B. V. Subba; Reddy, M. Ramana; Rao, Y. Gopal; Yadav; Sridhar
Organic Letters, 2013 , vol. 15, # 3 p. 464 - 467
反应条件
1.1: TiCl4 / CH2Cl2 / 0.5 h
1.2: CH2Cl2 / 1 h / -78 °C
View Scheme
参考文献
Yadav, Veejendra K.; Balamurugan, Rengarajan
Organic Letters, 2003 , vol. 5, # 23 p. 4281 - 4284
反应条件
potassium fluoride; 2,2'-azo-bisisobutyronitrile
1.) C6H6, reflux, 3 h, 2.) Et2O, r.t.; Yield given. Multistep reaction;
参考文献
Dang, Hai-Shan; Roberts, Brian P.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 769 - 775
反应条件
pyridine; Fe(III)TPPCl in chloroform
T=20°C; 7 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
(meso-tetraphenylporphyrin)Ru(CO) in dichloromethane
T=25°C; 24 h; Title compound not separated from byproducts.;
参考文献
Nicolas, Irene; Maux, Paul Le; Simonneaux, Gerard
Tetrahedron Letters, 2008 , vol. 49, # 13 p. 2111 - 2113
反应条件
pyridine; Halterman iron porphyrin in chloroform
T=40°C; optical yield given as percent deenantioselective reaction;
参考文献
Nicolas, Irene; Roisnel, Thierry; Maux, Paul Le; Simonneaux, Gerard
Tetrahedron Letters, 2009 , vol. 50, # 36 p. 5149 - 5151
反应条件
1: 2-diazo-1-phenylethanone; benzaldehyde With copper(l) iodide; triphenylphosphine in toluene
T=80°C; Inert atmosphere;
2: diazomethane With palladium diacetate in toluene
T=-78°C; Inert atmosphere; diastereoselective reaction;
参考文献
Davi, Michael; Lebel, Helene
Chemical Communications, 2008 , # 40 p. 4974 - 4976
反应条件
pyridine; Fe(III)TPPCl in chloroform
T=20°C; 7 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
