2-二氮杂-1-苯乙酮合成路线 (共 259 条)
反应条件
[(η5-C5H5)Ru(PPh3)2Cl] in chloroform-d1
T=60°C; Decomposition; cross coupling;
参考文献
Zotto, Alessandro Del; Baratta, Walter; Verardo, Giancarlo; Rigo, Pierluigi
European Journal of Organic Chemistry, 2000 , # 15 p. 2795 - 2802
反应条件
[(η5-C5H5)Ru(PPh3)2Cl] in chloroform-d1
T=60°C; Decomposition; cross coupling;
参考文献
Zotto, Alessandro Del; Baratta, Walter; Verardo, Giancarlo; Rigo, Pierluigi
European Journal of Organic Chemistry, 2000 , # 15 p. 2795 - 2802
反应条件
[(η5-C5H5)Ru(PPh3)2Cl] in chloroform-d1; hexane
T=60°C; Decomposition; cross coupling;
参考文献
Zotto, Alessandro Del; Baratta, Walter; Verardo, Giancarlo; Rigo, Pierluigi
European Journal of Organic Chemistry, 2000 , # 15 p. 2795 - 2802
反应条件
dirhodium tetraacetate
T=60°C; 1 h;
参考文献
Fukushima, Kazuaki; Ibata, Toshikazu
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 12 p. 3469 - 3482
反应条件
dirhodium tetraacetate; dimethyl acetylenedicarboxylate
T=60°C;
参考文献
Fukushima, Kazuaki; Ibata, Toshikazu
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 12 p. 3469 - 3482
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=80°C; 2 h;
参考文献
Yadav; Subba Reddy; Gopala Rao; Narsaiah
Chemistry Letters, 2008 , vol. 37, # 3 p. 348 - 349
反应条件
1: 90 percent / BF3*Et2O / diethyl ether / Ambient temperature
2: 98 percent / triethylamine / dimethylformamide / Heating
3: 1.) H2O, p-toluenesulfonic acid, 2.) periodic acid / 1.) CH3OH, reflux, 1 h, 2.) CH3OH, RT, 40 min
View Scheme
参考文献
Kachinsky, Joseph L. C.; Salomon, Robert G.
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1393 - 1401
反应条件
ethanol; platinum
Hydrogenation;
参考文献
Gruber; Renner
Monatshefte fuer Chemie, 1950 , vol. 81, p. 751,758
参考文献
Maier,G.
Chemische Berichte, 1962 , vol. 95, p. 611 - 615
Full Text Show Details
Grundmann
Justus Liebigs Annalen der Chemie, 1938 , vol. 536, p. 29,34
反应条件
Fe(III)TPPCl in dichloromethane
T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Nicolas, Irene; Roisnel, Thierry; Maux, Paul Le; Simonneaux, Gerard
Tetrahedron Letters, 2009 , vol. 50, # 36 p. 5149 - 5151