2-二氮杂-1-苯乙酮合成路线 （共 259 条）
参考文献
Bradley; Robinson
Journal of the American Chemical Society, 1930 , vol. 52, p. 1558,1562, 1563
反应条件
1: CH2Cl2 / 2 h / 20 °C 2: CH2Cl2 / 6 h 3: 82 percent / Et3N; p-TsCl / CH2Cl2 / 8 h / 20 °C View Scheme
参考文献
Aller, Enrique; Molina, Pedro; Lorenzo, Angeles
Synlett, 2000 , # 4 p. 526 - 528
反应条件
1: 82 percent / TsN3, KF 2: 80 percent / Al2O3 / pentane; diethyl ether View Scheme
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
反应条件
1: 98 percent / TsN3, KF 2: 26 percent / Al2O3 / pentane; diethyl ether View Scheme
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
反应条件
in methanol 1 h; Ambient temperature;
参考文献
Sezer, Oezkan; Anac, Olcay
Helvetica Chimica Acta, 1994 , vol. 77, # 8 p. 2323 - 2334
反应条件
diethyl ether T=-5 - 0°C;
参考文献
Bradley; Robinson
Journal of the Chemical Society, 1928 , p. 1316
Nature (London, United Kingdom), vol. 122, p. 130
反应条件
sodium nitrite Ansaeuern mit Essigsaeure;
参考文献
Angeli
Gazzetta Chimica Italiana, 1893 , vol. 23 II, p. 351
Gazzetta Chimica Italiana, 1894 , vol. 24 II, p. 318
反应条件
potassium permanganate
参考文献
Wolff
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 44
反应条件
lithium diisopropyl amide 1.) -30 deg C, 20 min, hexane, diethyl ether; 2.) -60 deg C to r.t., 1 h,diethyl ether; Multistep reaction;
参考文献
Sekiguchi, Akira; Sato, Takashi; Ando, Wataru
Chemistry Letters, 1983 , p. 1083 - 1084
反应条件
ethanol; potassium carbonate
参考文献
I.G. Farbenind.
Patent: DE724757 , 1940 ;
DRP/DRBP Org.Chem.
