2-二氮杂-1-苯乙酮合成路线 （共 259 条）
反应条件
in benzene T=40°C; 10 h; Irradiationother solvent cyclohexane; Product distribution;
参考文献
Rao, T. S. S.; Pritzkow, W.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 4 p. 617 - 625
参考文献
Wolff
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 44
反应条件
1: potassium dimethoxy(phenyl)(trifluoromethyl)borate With trimethylsilyl trifluoromethanesulfonate in ethylene glycol dimethyl ether T=-20 - -10°C; 0.333333 h; Inert atmosphere; 2: 2-diazo-1-phenylethanone With methanol in ethylene glycol dimethyl ether T=-20 - 20°C; 3 h; Inert atmosphere;
参考文献
Elkin, Pavel K.; Levin, Vitalij V.; Dilman, Alexander D.; Struchkova, Marina I.; Belyakov, Pavel A.; Arkhipov, Dmitry E.; Korlyukov, Alexander A.; Tartakovsky, Vladimir A.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5259 - 5263
反应条件
1: 81 percent / diethyl ether 2: 84 percent / SnCl4 / Ambient temperature 3: 88 percent / Zn / acetic acid View Scheme
参考文献
McKervey, M. Anthony; Ratananukul, Piniti
Tetrahedron Letters, 1983 , vol. 24, # 1 p. 117 - 120
反应条件
ethanol Irradiation.UV-Licht;
参考文献
Farbw. Hoechst
Patent: DE915214 , 1951 ;
反应条件
1: 79 percent / rhodium(II) acetate dimer / CH2Cl2 / 0.33 h / 25 °C 2: 62 percent / <ClRh(CO)2>2 / CH2Cl2 / 0.5 h / 25 °C View Scheme
参考文献
Padwa, Albert; Kassir, Jamal M.; Xu, Simon L.
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1642 - 1652
反应条件
In(OSO2CF3)3 T=20°C;
参考文献
Muthusamy, Sengodagounder; Babu, Srinivasarao Arulananda; Gunanathan, Chidambaram
Tetrahedron Letters, 2002 , vol. 43, # 17 p. 3133 - 3136
反应条件
diethyl ether Behandeln des Reaktionsprodukts mit wss. KOH;
参考文献
Weygand; Bestmann
Chemische Berichte, 1955 , vol. 88, p. 1992
反应条件
aluminium trichloride in neat (no solvent) T=25°C;
参考文献
Doyle, Michael P.; Buhro, William E.; Davidson, James G.; Elliott, Robert C.; Hoekstra, James W.; Oppenhuizen, Mark
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3657 - 3664
反应条件
dirhodium tetraacetate T=60°C; 1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 12 p. 3469 - 3482
