1-特-丁基-4-硝基苯合成路线 (共 81 条)
反应条件
1: Fe, aq. HCl 2: 1.) diazotization, 2.) KI View Scheme
参考文献
Kampmeier, J. A.; Nalli, Thomas W.
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1381 - 1388
反应条件
1: nitric acid / 60 °C 2: alcohol; hydrogen sulfide; ammonia 3: absolute-alcoholic sulfuric acid / Diazotization View Scheme
参考文献
Shoesmith; Mackie
Journal of the Chemical Society, 1928 , p. 2336
反应条件
dirhodium tetraacetate in toluene T=80°C; 7 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 23 p. 3116 - 3118
反应条件
formic acid; iron(II) chloride heptahydrate; triethylamine T=150°C; 12 h;
参考文献
Jiang, Xue; Wang, Chao; Wei, Yawen; Xue, Dong; Liu, Zhaotie; Xiao, Jianliang
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 58 - 63
反应条件
1: H2 / Pd/C / ethanol 2: 2 h / 110 °C 3: fuming nitric acid / 0 - 5 °C 4: 9 M HCl / 0.5 h / Heating View Scheme
参考文献
Kuhler; Fryklund; Bergman; Weilitz; Lee; Larsson
Journal of Medicinal Chemistry, 1995 , vol. 38, # 25 p. 4906 - 4916
反应条件
2: 30 percent / As2O5, conc. H2SO4 View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: H2 / Pd/C / ethanol 2: 2 h / 110 °C 3: fuming nitric acid / 0 - 5 °C 4: 9 M HCl / 0.5 h / Heating 5: H2 / Pd/C / ethanol View Scheme
参考文献
Kuhler; Fryklund; Bergman; Weilitz; Lee; Larsson
Journal of Medicinal Chemistry, 1995 , vol. 38, # 25 p. 4906 - 4916
反应条件
1: nitric acid / 60 °C 2: alcohol; hydrogen sulfide; ammonia 3: absolute-alcoholic sulfuric acid / Diazotization 4: iron; acetic acid / 90 °C View Scheme
参考文献
Shoesmith; Mackie
Journal of the Chemical Society, 1928 , p. 2336
反应条件
γ-terpinene in ethanol T=80°C; 0.75 h; Sealed tubeGreen chemistry;
参考文献
Verho, Oscar; Nagendiran, Anuja; Tai, Cheuk-Wai; Johnston, Eric V.; Baeckvall, Jan-E.
ChemCatChem, 2014 , vol. 6, # 1 p. 205 - 211
反应条件
hydrogenchloride; iron unter Luftzutritt;
参考文献
Crawford; Stewart
Journal of the Chemical Society, 1952 , p. 4443,4445