1-特-丁基-4-硝基苯合成路线 （共 81 条）
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-40°C; 0.00416667 h; Inert atmosphere;
参考文献
Blazej, Sylwia; Makosza, Mieczyslaw
Chemistry - A European Journal, 2008 , vol. 14, # 35 p. 11113 - 11122
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-40°C; 0.00416667 h; Inert atmosphere;
参考文献
Blazej, Sylwia; Makosza, Mieczyslaw
Chemistry - A European Journal, 2008 , vol. 14, # 35 p. 11113 - 11122
反应条件
1: H2 / Raney-Ni
2: (i) aq. HCl, (ii) NaNO2, aq. HBF4, (iii) (thermolysis)
View Scheme
参考文献
Ruechardt,C.; Eichler,S.
Chemische Berichte, 1962 , vol. 95, p. 1921 - 1942
反应条件
1: Cl2, Ag2SO4, H2SO4
2: H2 / Raney-Ni
3: (i) NaNO2, (ii) H3PO2
View Scheme
参考文献
Ruechardt,C.; Eichler,S.
Chemische Berichte, 1962 , vol. 95, p. 1921 - 1942
反应条件
1: dibromoisocyanuric acid, aq. H2SO4
2: (i) EtOH, aq. HCl, (electrochemical reduction), (ii) aq. NaNO2, (iii) aq. H3PO2
View Scheme
参考文献
Lamm,B.; Ankner,K.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1977 , vol. 31, p. 375 - 381
反应条件
2: 30 percent / As2O5, conc. H2SO4
3: hydrogen / platinum oxide / methanol / 2250.2 Torr
View Scheme
参考文献
Hoenel, Michael; Vierhapper, Friedrich W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1933 - 1939
反应条件
1: zinc, ammonium chloride
2: sodium dichromate, sulphuric acid
View Scheme
参考文献
Al-Tahou, Baheeja M.; Gowenlock, Brian G.
Recueil des Travaux Chimiques des Pays-Bas, 1986 , vol. 105, p. 353 - 355
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-40°C; 0.00416667 h; Inert atmosphere;
参考文献
Blazej, Sylwia; Makosza, Mieczyslaw
Chemistry - A European Journal, 2008 , vol. 14, # 35 p. 11113 - 11122
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-40°C; 0.00416667 h; Inert atmosphere;
参考文献
Blazej, Sylwia; Makosza, Mieczyslaw
Chemistry - A European Journal, 2008 , vol. 14, # 35 p. 11113 - 11122
反应条件
potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=-40°C; 0.00416667 h; Inert atmosphere;
参考文献
Blazej, Sylwia; Makosza, Mieczyslaw
Chemistry - A European Journal, 2008 , vol. 14, # 35 p. 11113 - 11122
