5-溴甲基-2,1,3-苯并二唑合成路线 （共 5 条）
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane 6 h; Heating;
参考文献
D'yachenko, S. A.; Bureneva, M. I.; Papirnik, M. P.; Pesin, V. G.; Ostashkova, N. V.; Stetsenko, A. I.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 8 p. 1912 - 1919,1642 - 1648
反应条件
1: triethyl phosphite / ethanol / 0.5 h / Heating 2: N-bromosuccinimide; benzoyl peroxide / CCl4 / 18 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 6 p. 899 - 908
反应条件
1: toluene / 2 h / Heating 2: triethyl phosphite / ethanol / 0.5 h / Heating 3: N-bromosuccinimide; benzoyl peroxide / CCl4 / 18 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 6 p. 899 - 908
反应条件
1: 74 percent / water, calcium carbonate / dioxane / 3 h / Heating 2: 91 percent / manganese dioxide / CHCl3 / 2 h / Ambient temperature View Scheme
参考文献
Gasco; Ermondi; Fruttero
European Journal of Medicinal Chemistry, 1996 , vol. 31, # 1 p. 3 - 10
反应条件
water; calcium carbonate in 1,4-dioxane
3 h; Heating;
参考文献
Gasco; Ermondi; Fruttero
European Journal of Medicinal Chemistry, 1996 , vol. 31, # 1 p. 3 - 10
