1-甲基-4-苯基乙炔苯合成路线 （共 165 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride in 1,2-dichloro-ethane T=20°C; 5 h; Title compound not separated from byproducts;
参考文献
Kakusawa, Naoki; Tobiyasu, Yoshinori; Yasuike, Shuji; Yamaguchi, Kentaro; Seki, Hiroko; Kurita, Jyoji
Tetrahedron Letters, 2003 , vol. 44, # 47 p. 8589 - 8592
反应条件
PhCH2Pd(PPh3)2Cl in 1,2-dichloro-ethane T=20°C; 0.0833333 h;
参考文献
Kakusawa, Naoki; Tobiyasu, Yoshinori; Yasuike, Shuji; Yamaguchi, Kentaro; Seki, Hiroko; Kurita, Jyoji
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 2953 - 2968
反应条件
PhCH2Pd(PPh3)2Cl in 1,2-dichloro-ethane T=20°C; 0.0833333 h;
参考文献
Kakusawa, Naoki; Tobiyasu, Yoshinori; Yasuike, Shuji; Yamaguchi, Kentaro; Seki, Hiroko; Kurita, Jyoji
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 2953 - 2968
反应条件
1: 1,2-dimethoxy-ethane; tetrahydrofuran; hexane / 2.5 h / -78 - 20 °C 2: 96 percent / Pd(PPh3)4 / 1,2-dimethoxy-ethane; tetrahydrofuran; hexane / 2 h / 80 °C View Scheme
参考文献
Castanet, Anne-Sophie; Colobert, Francoise; Schlama, Thierry
Organic Letters, 2000 , vol. 2, # 23 p. 3559 - 3561
反应条件
2: 95 percent / KOH View Scheme
参考文献
Tartaggia, Stefano; De Lucchi, Ottorino; Goossen, Lukas J.
European Journal of Organic Chemistry, 2012 , # 7 p. 1431 - 1438
反应条件
palladium diacetate in toluene T=70°C; Addition; 20 h;
参考文献
Granier; Cardenas; Echavarren
Tetrahedron Letters, 2000 , vol. 41, # 35 p. 6775 - 6779
反应条件
PhCH2Pd(PPh3)2Cl in 1,2-dichloro-ethane T=80°C; 5 h;
参考文献
Kakusawa, Naoki; Tobiyasu, Yoshinori; Yasuike, Shuji; Yamaguchi, Kentaro; Seki, Hiroko; Kurita, Jyoji
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 2953 - 2968
反应条件
PhCH2Pd(PPh3)2Cl in 1,2-dichloro-ethane T=20°C; 0.0833333 h;
参考文献
Kakusawa, Naoki; Tobiyasu, Yoshinori; Yasuike, Shuji; Yamaguchi, Kentaro; Seki, Hiroko; Kurita, Jyoji
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 2953 - 2968
反应条件
potassium fluoride; 18-crown-6 ether; copper(l) chloride in tetrahydrofuran T=50°C; 5.5 h; Inert atmosphere;
参考文献
Yoshida, Hiroto; Morishita, Takami; Nakata, Hiromi; Ohshita, Joji
Organic Letters, 2009 , vol. 11, # 2 p. 373 - 376
反应条件
1: 2,6-lutidine / CH2Cl2 / 0 - 20 °C 2: 2N NaOH / tetrahydrofuran / 1 h / 20 °C 3: 51 percent / toluene; tetrahydrofuran / -45 - 20 °C View Scheme
参考文献
Katritzky, Alan R.; Abdel-Fattah, Ashraf A. A.; Wang, Mingyi
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7526 - 7529
