1-甲基-4-苯基乙炔苯合成路线 （共 165 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 0.5 h; Heating;
参考文献
Perez; Sestelo; Sarandeses
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4155 - 4160
反应条件
C32H28BrFeIN3Pd; potassium acetate; silver(l) oxide in 1,2-dichloro-ethane T=80°C; 24 h;
参考文献
Li, Hong-Mei; Xu, Chen; Duan, Lu-Meng; Lou, Xin-Hua; Wang, Zhi-Qiang; Li, Zhen; Fan, Yao-Ting
Transition Metal Chemistry, 2013 , vol. 38, # 3 p. 313 - 318
反应条件
2,6-di-tert-butyl-4-methylpyridine; gold(I) chloride; palladium dichloride; SIDip*HCl in acetonitrile T=20°C; Sonogashira coupling;
参考文献
Panda, Biswajit; Sarkar, Tarun K.
Chemical Communications, 2010 , vol. 46, # 18 p. 3131 - 3133
反应条件
tert.-butylnitrite; trifuran-2-yl-phosphane; palladium diacetate; acetic acid in dimethyl sulfoxide T=20 - 32°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2011 , vol. 47, # 28 p. 7959 - 7961
反应条件
Cu(I) 3-methylsalicylate; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=45 - 50°C; Sonogashira coupling; 22 h;
参考文献
Henke, Adam; Srogl, Jiri
Chemical Communications, 2011 , vol. 47, # 14 p. 4282 - 4284
反应条件
copper(l) chloride; palladium dichloride; tris(p-fluoro phenyl)phosphine in N,N-dimethyl-formamide T=100°C; sila-Sonogashira-Hagihara cross-coupling; 12 h; Inert atmosphere;
参考文献
Nishihara, Yasushi; Inoue, Eiji; Noyori, Shintaro; Ogawa, Daisuke; Okada, Yoshiaki; Iwasaki, Masayuki; Takagi, Kentaro
Tetrahedron, 2012 , vol. 68, # 24 p. 4869 - 4881
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=20°C; Substitution; 24 h;
参考文献
Chang Ho Oh; Seung Hyun Jung
Tetrahedron Letters, 2000 , vol. 41, # 44 p. 8513 - 8516
反应条件
1: Sb(o-tolyl)3 With [bis(acetoxy)iodo]benzene in dichloromethane T=20°C; 7 h; 2: 1-trimethylsilyl-2-phenylacetylene With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(l) iodide in acetonitrile T=50°C; 5 h; Further stages.;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Hong, Young-Taek
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 7 p. 736 - 739
反应条件
copper(l) iodide; sodium methylate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in methanol; acetonitrile T=20°C;
参考文献
Kang; Ryu; Lee
Synthetic Communications, 2001 , vol. 31, # 7 p. 1059 - 1064
反应条件
t-Bu2P(biphenyl); tetrabutyl ammonium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran T=20°C; 24 h;
参考文献
Faller, Jack W.; Kultyshev, Roman G.; Parr, Jonathan
Tetrahedron Letters, 2003 , vol. 44, # 3 p. 451 - 453
