3-乙基-2-丙基-喹啉合成路线 (共 42 条)
反应条件
1: With potassium hydroxide; copper dichloride in 1,4-dioxane T=20°C; 2: With oxygen in 1,4-dioxane Reflux;
参考文献
Wang, Tianli; Zhuo, Lian-Gang; Li, Zhiwei; Chen, Fei; Ding, Ziyuan; He, Yanmei; Fan, Qing-Hua; Xiang, Junfeng; Yu, Zhi-Xiang; Chan, Albert S. C.
Journal of the American Chemical Society, 2011 , vol. 133, # 25 p. 9878 - 9891
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in toluene T=180°C; 20 h;
参考文献
Cho, Chan Sik; Lee, Na Young; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 3 p. 423 - 429
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in toluene T=180°C; 20 h;
参考文献
Cho, Chan Sik; Lee, Na Young; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 3 p. 423 - 429
反应条件
1: benzaldehyde; aniline With [IrHCl2(cod)]2 in dimethyl sulfoxide T=20°C; Mannich reaction; 1 h; 2: butyraldehyde With air in dimethyl sulfoxide T=90°C; 12 h;
参考文献
Nakajima, Takayuki; Inada, Takashi; Igarashi, Takeyuki; Sekioka, Tadashi; Shimizu, Isao
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 12 p. 1941 - 1949
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; P(C4H9)3 in ethanol T=180°C; P=53200 Torr; 4 h;
参考文献
Watanabe, Yoshihisa; Suzuki, Naoki; Tsuji, Yasushi; Shim, Sang Chul; Mitsudo, Take-aki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1116 - 1120
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in dimethyl sulfoxide T=90°C; 17 h;
参考文献
Igarashi, Takeyuki; Inada, Takashi; Sekioka, Tadao; Nakajima, Takayuki; Shimizu, Isao
Chemistry Letters, 2005 , vol. 34, # 1 p. 106 - 107
反应条件
palladium on activated charcoal T=230°C;
参考文献
Nielsen et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 4696,4700
反应条件
1: benzaldehyde; aniline With [IrHCl2(cod)]2 in dimethyl sulfoxide T=20°C; Mannich reaction; 1 h; 2: butyraldehyde With oxygen in dimethyl sulfoxide T=90°C; 12 h;
参考文献
Dzhemilev, U. M.; Selimov, F. A.; Khusnutdinov, R. A.; Fatykhov, A. A.; Khalilov, L. M.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 6.2 p. 1248 - 1253
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 6 p. 1407 - 1413
反应条件
carbon monoxide; RhCl(PPh3)3; palladium dichloride in ethanol; water T=180°C; 4 h;
参考文献
Watanabe, Yoshihisa; Suzuki, Naoki; Shim, Sang Chul; Yamamoto, Michihiro; Mitsudo, Take-aki; Takegami, Yoshinobu
Chemistry Letters, 1980 , p. 429 - 430
反应条件
nitrobenzene; ruthenium trichloride in benzene T=180°C; 4 h; high pressure;
参考文献
Watanabe; Tsuji; Shida
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 435 - 438