2-甲基-3-苯基-1-丙烯合成路线 (共 66 条)
反应条件
dicobalt octacarbonyl in benzene T=140°C; P=38000 Torr;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 7361
反应条件
magnesium in tetrahydrofuran
参考文献
Botes, Adriana Leonora; Lotter, Jeanette
Patent: US2008/286832 A1, 2008 ;
反应条件
triphenyl phosphite; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in toluene T=100°C; Suzuki-Miyaura coupling; 1 h;
参考文献
Kayaki, Yoshihito; Koda, Takashi; Ikariya, Takao
European Journal of Organic Chemistry, 2004 , # 24 p. 4989 - 4993
反应条件
palladium (II) trifluoroacetate; potassium hydroxide in water T=90°C; Suzuki Coupling; 3 h; Green chemistry;
参考文献
Dong, Chaonan; Zhang, Lingjuan; Xue, Xiao; Li, Huanrong; Yu, Zhiyong; Tang, Weijun; Xu, Lijin
RSC Advances, 2014 , vol. 4, # 22 p. 11152 - 11158
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 1 h;
参考文献
Hirabe, Tomoatsu; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4084 - 4086
反应条件
potassium hydroxide; C16H16Cl2N2O4Pd2; tetrabutylammomium bromide in water; acetone T=50°C; 2 h; DarknessInert atmosphere;
参考文献
Alacid, Emilio; Najera, Carmen
Organic Letters, 2008 , vol. 10, # 21 p. 5011 - 5014
反应条件
para-dicyanobenzene; 2,4,6-trimethyl-pyridine; biphenyl in acetonitrile T=10°C; Irradiation;
参考文献
Arnold, Donald R.; Mines, Shelley A.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 689 - 698
反应条件
Pd0(tris(tert-butyl)phosphine)2 in tetrahydrofuran T=25°C; 0.5 h; Inert atmosphere; regioselective reaction;
参考文献
Rao Volla, Chandra M.; Dubbaka, Srinivas Reddy; Vogel, Pierre
Tetrahedron, 2009 , vol. 65, # 2 p. 504 - 511
反应条件
chloro-trimethyl-silane; Cu(I)[(CH3CN)4]BF4 in tetrahydrofuran T=0°C;
参考文献
Deshmukh; Jadhav, Sunil; Anbhule; Mali; Suryawanshi
Journal of Chemical Research, 2006 , # 4 p. 248 - 250
反应条件
Pd0(tris(tert-butyl)phosphine)2 in tetrahydrofuran T=25°C; 0.5 h; Inert atmosphere; regioselective reaction;
参考文献
Rao Volla, Chandra M.; Dubbaka, Srinivas Reddy; Vogel, Pierre
Tetrahedron, 2009 , vol. 65, # 2 p. 504 - 511