3,4,5-三甲氧基苯甲酰肼合成路线 （共 37 条）
反应条件
1: 95 percent / ethanol / 1 h / Heating 2: 73 percent / POCl3 / 1 h / Heating View Scheme
参考文献
Al-Omar, Mohamed; Al-Deeb, Omar A.; Al-Khamees, Hamad A.; El-Emam, Ali A.
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 12 p. 2509 - 2517
参考文献
Kalb; Gross
Chemische Berichte, 1926 , vol. 59, p. 733
参考文献
Nakata; Nishihara
Yakugaku Zasshi, 1944 , vol. 64, # 2 p. 74
Chem.Abstr., 1951 , p. 2955
反应条件
1: potassium hydroxide / ethanol / 3 h / 25 °C 2: hydrazine hydrate / H2O / 1 h / Heating 3: hydrazine hydrate / H2O / 1 h / Heating View Scheme
参考文献
Sung; Lee
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1101 - 1109
反应条件
1: potassium hydroxide / ethanol / 3 h / 25 °C
2: hydrazine hydrate / H2O / 1 h / Heating
3: hydrazine hydrate / H2O / 1 h / Heating
4: 96 percent / potassium carbonate / acetone / 10 h / Heating
5: 63 percent / aq. sodium hydroxide / 4 h / Heating
View Scheme
参考文献
Sung; Lee
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1101 - 1109
参考文献
Buchanan; Cook; Loudon
Journal of the Chemical Society, 1944 , p. 325,327
反应条件
1: 85 percent / 1 h / Heating
2: 85 percent / 5percent NaOH / H2O / 4 h / Heating
View Scheme
参考文献
Sung; Lee
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1101 - 1109
反应条件
1: 75 percent / 1 h / Heating
2: 75 percent / 5percent NaOH / H2O / 4 h / Heating
View Scheme
参考文献
Mazzone; Bonina; Reina; Blandino
Farmaco, Edizione Scientifica, 1981 , vol. 36, # 3 p. 181 - 196
反应条件
1: 90 percent / 1 h / Heating
2: 90 percent / 5percent NaOH / H2O / 4 h / Heating
3: 75 percent / 1/10 N NaOH / H2O / 2 h / Heating
View Scheme
参考文献
Mazzone; Bonina; Reina; Blandino
Farmaco, Edizione Scientifica, 1981 , vol. 36, # 3 p. 181 - 196
反应条件
1: 90 percent / 1 h / Heating
2: 90 percent / 5percent NaOH / H2O / 4 h / Heating
3: 75 percent / 1/10 N NaOH / H2O / 2 h / Heating
4: 62 percent / acetic acid anhydride / 2 h / Heating
View Scheme
参考文献
Mazzone; Bonina; Reina; Blandino
Farmaco, Edizione Scientifica, 1981 , vol. 36, # 3 p. 181 - 196
