7-甲基-1,4-二噁螺[4.5]-7-癸烯-8-羧酸乙酯合成路线 （共 4 条）
反应条件
toluene-4-sulfonic acid in benzene 12 h; Heating;
参考文献
Fulmer, T. D.; Bryson, T. A.
Journal of Organic Chemistry, 1989 , vol. 54, p. 3496 - 3500
反应条件
toluene-4-sulfonic acid in toluene 5 h; Heating;
参考文献
Bezborodov, V. S.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1148 - 1152
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1268 - 1273
反应条件
hydrogenchloride; sodium hydroxide; nitrogen in tetrahydrofuran
参考文献
The Board of Trustees of Leland Stanford Junior University
Patent: US4055603 A1, 1977 ;
反应条件
hydrogenchloride; sodium bis(2-methoxyethoxy)aluminium dihydride
1.) benzene, THF, room temperature, overnight, 2.) water, room temperature, 4 h; Yield given. Multistep reaction;
参考文献
Johnson, William S.; McCarry, Brian E.; Markezich, R. L.; Boots, Sharon G.
Journal of the American Chemical Society, 1980 , vol. 102, # 1 p. 352 - 359
