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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-吡啶硼酸频哪醇酯
合成路线
（共 42 条）
38749-79-0
2-甲基-3-溴吡啶
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
1214326-04-1
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
536-74-3
苯乙炔
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
13238-38-5
3-苯基乙炔吡啶
反应条件
potassium acetate; silver(l) oxide in dichloromethane T=20°C; 24 h;
参考文献
Yang, Fan; Wu, Yangjie
European Journal of Organic Chemistry, 2007 , # 21 p. 3476 - 3479
24424-99-5
二碳酸二叔丁酯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
65321-36-0
反应条件
palladium diacetate; triphenylphosphine in 1,4-dioxane T=100°C; 15 h; Inert atmosphere; Reagent/catalystSolventTemperature;
参考文献
Wu, Yusheng; Li, Xinjian; Zou, Dapeng; Zhu, Helong; Wang, Yaping; Li, Jingya; Wu, Yangjie
Organic Letters, 2014 , vol. 16, # 7 p. 1836 - 1839
799293-91-7
3-溴-7-碘-噻吩并[3,2-c]吡啶-4-胺
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
832696-86-3
3-溴-7-(3-吡啶)-噻吩并[3,2-c]吡啶-4-胺
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; N,N-dimethyl-formamide T=120°C; 0.25 h; Microwave;
参考文献
Tang, Jun; Lackey, Karen E.; Dickerson, Scott H.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 1 p. 66 - 70
26163-07-5
5-溴-2-二甲基氨基吡啶
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
882864-93-9
反应条件
potassium phosphate; (C5H5FeC5H3C(CH3)NC6H4CH3)PdCl(tricyclohexylphosphine); potassium acetate in 1,4-dioxane; water T=100°C; Suzuki coupling; 15 h; Inert atmosphere;
参考文献
Wang, Lianhui; Cui, Xiuling; Li, Jingya; Wu, Yusheng; Zhu, Zhiwu; Wu, Yangjie
European Journal of Organic Chemistry, 2012 , # 3 p. 595 - 603
13329-40-3
4-碘代苯乙酮
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 10 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
99-90-1
4-溴苯乙酮
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
90395-45-2
4-(3-吡啶)苯甲醛
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 6 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
95-46-5
邻溴甲苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
90395-49-6
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 10 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
95-49-8
2-氯甲苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
90395-49-6
反应条件
caesium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 24 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
402-43-7
对溴三氟甲苯
+
329214-79-1
3-吡啶硼酸频哪醇酯
→
反应条件
426823-25-8
3-[4-(三氟甲基）苯基]吡啶
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide T=110°C; Suzuki cross-coupling reaction; 10 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
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