1,2,3,4-四氢吖啶合成路线 （共 54 条）
反应条件
1: 71 percent / copper(I) iodide; Cu powder / PdCl2(dppf)2*CH2Cl2 / dimethylsulfoxide / 2 h / 90 °C 2: 46 percent / H2 / Pd/C / methanol / 2 h / 18 °C / 760 Torr View Scheme
参考文献
Organic Letters, , vol. 6, # 16 p. 2741 - 2744
反应条件
1: 71 percent / copper(I) iodide; Cu powder / PdCl2(dppf)2*CH2Cl2 / dimethylsulfoxide / 2 h / 90 °C 2: 46 percent / H2 / Pd/C / methanol / 2 h / 18 °C / 760 Torr View Scheme
参考文献
Organic Letters, , vol. 6, # 16 p. 2741 - 2744
反应条件
iron in acetic acid 2 h; Reflux;
参考文献
Ramesh, Chintakunta; Kavala, Veerababurao; Kuo, Chun-Wei; Yao, Ching-Fa
Tetrahedron Letters, 2010 , vol. 51, # 40 p. 5234 - 5237
反应条件
in aqueous potassium hydroxide; ethanol; water; cyclohexanone
反应条件
iron in acetic acid 2 h; Reflux;
参考文献
Ramesh, Chintakunta; Kavala, Veerababurao; Kuo, Chun-Wei; Yao, Ching-Fa
Tetrahedron Letters, 2010 , vol. 51, # 40 p. 5234 - 5237
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol 20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
sulfur dioxide; methylamine in water T=120 - 140°C; 20 h; in a sealed ampul;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 18, # 10 p. 1065 - 1071
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 18, # 10 p. 1374 - 1380
反应条件
T=750°C; P=0.01 Torr;
参考文献
Mao, Yuh-lin; Boekelheide, V.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1547 - 1548
反应条件
in tetrahydrofuran Heating;
参考文献
Katritzky, Alan R.; Arend, Michael
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9989 - 9991
反应条件
1: 92 percent / p-Toluenesulfonic acid / benzene / Heating; Continuous removal of water 2: 42 percent / 750 °C / 0.01 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 8 p. 1547 - 1548
