2-吡啶-2-基-1,3-苯并恶唑合成路线 （共 26 条）
反应条件
1: DBU / PdCl2(PPh3)2, PPh3 / toluene / 1.25 h / 120 °C / 4654.3 Torr 2: methanesulfonic acid / toluene / 2 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 10 p. 2883 - 2887
反应条件
1: DBU / PdCl2(PPh3)2, PPh3 / toluene / 1.25 h / 120 °C / 4654.3 Torr 2: methanesulfonic acid / toluene / 2 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 10 p. 2883 - 2887
反应条件
T=800°C; P=0.001 Torr; 8.33333E-06 h; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 12 p. 4352 - 4358
反应条件
sulfur T=160 - 170°C; 10 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 8 p. 2996 - 3004
反应条件
2,6-di-tert-butyl-4-methylpyridine; thianthrene cation radical perchlorate in acetonitrile T=20°C;
参考文献
Journal of Heterocyclic Chemistry, , vol. 39, # 6 p. 1279 - 1281
反应条件
methanesulfonic acid in 1,4-dioxane T=100°C; 2 h; chemoselective reaction;
参考文献
Australian Journal of Chemistry, , vol. 61, # 11 p. 881 - 887
反应条件
methanesulfonic acid in toluene 2 h; Heating; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 10 p. 2883 - 2887
反应条件
palladium dichloride in chlorobenzene Reflux;
参考文献
Green Chemistry, , vol. 16, # 4 p. 2132 - 2135
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 70, # 13 p. 5190 - 5196
反应条件
1: thionyl chloride / 1 h / Reflux 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C 3: potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; dcype / 1,4-dioxane / 24 h / 150 °C / Inert atmosphere; 8-well reaction block View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 33 p. 13573 - 13576
