3-(2-氧代环戊基)丙酸合成路线 （共 13 条）
反应条件
1: 1.) NaBH4 2.) aq. HCl
2: DIBAL
3: 2.) Jones oxidation
View Scheme
参考文献
Tanaka, Masakazu; Suemune, Hiroshi; Sakai, Kiyoshi
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1733 - 1736
反应条件
1: 80 percent / p-toluenesulfonic acid, acetic anhydride / benzene / 4 h / 0 °C
2: Br2 / CCl4 / 0.5 h / 0 °C
3: aq. NaHCO3 / CCl4 / 10 h
4: 51 percent / CH3SO3H, P2O5 / 2 h / 60 °C
View Scheme
参考文献
Mandal, A.K.; Jawalkar, D.G.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2364 - 2369
反应条件
1: 80 percent / p-toluenesulfonic acid, acetic anhydride / benzene / 4 h / 0 °C
2: Br2 / CCl4 / 0.5 h / 0 °C
3: aq. NaHCO3 / CCl4 / 10 h
View Scheme
参考文献
Mandal, Arun K.; Jawalkar, D. G.
Tetrahedron Letters, 1986 , vol. 27, # 1 p. 99 - 100
