5-硝基-2-(环氧乙烷基甲氧基)苯乙酮合成路线 （共 6 条）
反应条件
potassium carbonate in acetone T=60°C; 12 h;
参考文献
Dey, Sangeeta; Powell, Douglas R.; Hu, Chunhua; Berkowitz, David B.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 37 p. 7010 - 7014
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate T=75°C; 10 h;
参考文献
Joshi, Ramesh A.; Gurjar, Mukund K.; Tripathy, Narendra K.; Chorghade, Mukund S.
Organic Process Research and Development, 2001 , vol. 5, # 2 p. 176 - 178
反应条件
1: sodium hydroxide / water / 0.17 h / 90 - 95 °C 2: AlCl3, aluminium chloride / nitrobenzene / 6.5 h / 20 - 140 °C 3: potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride / 10 h / 75 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 5, # 2 p. 176 - 178
反应条件
1: AlCl3, aluminium chloride / nitrobenzene / 6.5 h / 20 - 140 °C 2: potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride / 10 h / 75 °C View Scheme
参考文献
Organic Process Research and Development, , vol. 5, # 2 p. 176 - 178
反应条件
1: water / 12 h / 20 °C 2: palladium 10 on activated carbon; hydrogen / methanol / 20 °C / 1034.32 Torr 3: triethylamine / tetrahydrofuran / 48 h / 40 °C 4: hydrogenchloride / acetone / 1.5 h / 20 °C / pH 5.5 - 6 View Scheme
参考文献
Joshi, Ramesh A.; Gurjar, Mukund K.; Tripathy, Narendra K.; Chorghade, Mukund S.
Organic Process Research and Development, 2001 , vol. 5, # 2 p. 176 - 178
反应条件
1: water / 12 h / 20 °C 2: palladium 10 on activated carbon; hydrogen / methanol / 20 °C / 1034.32 Torr 3: triethylamine / tetrahydrofuran / 48 h / 40 °C View Scheme
参考文献
Joshi, Ramesh A.; Gurjar, Mukund K.; Tripathy, Narendra K.; Chorghade, Mukund S.
Organic Process Research and Development, 2001 , vol. 5, # 2 p. 176 - 178
