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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
32976-84-4
合成路线
（共 10 条）
34793-14-1
→
反应条件
32976-84-4
反应条件
ammonia in methanol
参考文献
Morisawa, Hirokazu; Utagawa, Takashi; Miyoshi, Takeshi; Yoshinaga, Fumihiro; Yamazaki, Akihiro; Mitsugi, Koji
Tetrahedron Letters, 1980 , vol. 21, p. 479 - 482
120595-74-6
→
反应条件
32976-84-4
反应条件
sodium hydrogensulfide in ethanol 6 h; Heating;
参考文献
Hanna; Ramasamy; Robins; Revankar
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 6 p. 1899 - 1903
74491-89-7
→
反应条件
32976-84-4
反应条件
1: 72 percent / phosphorus pentasulfide / pyridine / 4 h / Heating 2: 60 percent / ammonia / methanol View Scheme
参考文献
Morisawa, Hirokazu; Utagawa, Takashi; Miyoshi, Takeshi; Yoshinaga, Fumihiro; Yamazaki, Akihiro; Mitsugi, Koji
Tetrahedron Letters, 1980 , vol. 21, p. 479 - 482
3083-77-0
阿糖尿苷
→
反应条件
32976-84-4
反应条件
1: 34 percent / 12 h / 60 °C / Enterobactor aerogenes, potassium phosphate buffer, (pH 7.0) 2: 85 percent / ammonia / methanol / 4 h / 150 °C 3: 88 percent / pyridine 4: 72 percent / phosphorus pentasulfide / pyridine / 4 h / Heating 5: 60 percent / ammonia / methanol View Scheme
参考文献
Morisawa, Hirokazu; Utagawa, Takashi; Miyoshi, Takeshi; Yoshinaga, Fumihiro; Yamazaki, Akihiro; Mitsugi, Koji
Tetrahedron Letters, 1980 , vol. 21, p. 479 - 482
70284-18-3
→
反应条件
32976-84-4
反应条件
1: 85 percent / ammonia / methanol / 4 h / 150 °C 2: 88 percent / pyridine 3: 72 percent / phosphorus pentasulfide / pyridine / 4 h / Heating 4: 60 percent / ammonia / methanol View Scheme
参考文献
Morisawa, Hirokazu; Utagawa, Takashi; Miyoshi, Takeshi; Yoshinaga, Fumihiro; Yamazaki, Akihiro; Mitsugi, Koji
Tetrahedron Letters, 1980 , vol. 21, p. 479 - 482
38819-10-2
9-β-D-糖呋喃鸟嘌呤
→
反应条件
32976-84-4
反应条件
1: 88 percent / pyridine 2: 72 percent / phosphorus pentasulfide / pyridine / 4 h / Heating 3: 60 percent / ammonia / methanol View Scheme
参考文献
Morisawa, Hirokazu; Utagawa, Takashi; Miyoshi, Takeshi; Yoshinaga, Fumihiro; Yamazaki, Akihiro; Mitsugi, Koji
Tetrahedron Letters, 1980 , vol. 21, p. 479 - 482
13368-14-4
2-氯-6-羟基嘌呤
→
反应条件
32976-84-4
反应条件
1: 34 percent / 12 h / 60 °C / Enterobactor aerogenes, potassium phosphate buffer, (pH 7.0) 2: 85 percent / ammonia / methanol / 4 h / 150 °C 3: 88 percent / pyridine 4: 72 percent / phosphorus pentasulfide / pyridine / 4 h / Heating 5: 60 percent / ammonia / methanol View Scheme
参考文献
Morisawa, Hirokazu; Utagawa, Takashi; Miyoshi, Takeshi; Yoshinaga, Fumihiro; Yamazaki, Akihiro; Mitsugi, Koji
Tetrahedron Letters, 1980 , vol. 21, p. 479 - 482
4060-34-8
1-氯-2,3,5-三-O-苄基-D-阿拉伯呋喃糖
→
反应条件
32976-84-4
反应条件
1: 1) sodium hydride (60percent in oil) / 1) acetonitrile, RT, 30 min; 2) acetonitrile, RT, 15 h 2: 62 percent / boron trichloride / CH2Cl2 / 1) -78 deg C, 4 h; 2) from -20 deg C to -30 deg C, 2 h 3: 74 percent / sodium hydrosulfide hydrate / ethanol / 6 h / Heating View Scheme
参考文献
Hanna; Ramasamy; Robins; Revankar
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 6 p. 1899 - 1903
35085-24-6
→
反应条件
32976-84-4
反应条件
1: 62 percent / boron trichloride / CH2Cl2 / 1) -78 deg C, 4 h; 2) from -20 deg C to -30 deg C, 2 h 2: 74 percent / sodium hydrosulfide hydrate / ethanol / 6 h / Heating View Scheme
参考文献
Hanna; Ramasamy; Robins; Revankar
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 6 p. 1899 - 1903
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
32976-84-4
反应条件
1: 1) sodium hydride (60percent in oil) / 1) acetonitrile, RT, 30 min; 2) acetonitrile, RT, 15 h 2: 62 percent / boron trichloride / CH2Cl2 / 1) -78 deg C, 4 h; 2) from -20 deg C to -30 deg C, 2 h 3: 74 percent / sodium hydrosulfide hydrate / ethanol / 6 h / Heating View Scheme
参考文献
Hanna; Ramasamy; Robins; Revankar
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 6 p. 1899 - 1903
