N,N'-二环己基草酰胺合成路线 (共 19 条)
反应条件
carbon monoxide in tetrahydrofuran; diethyl ether addn. of RNH2 to suspn. of complex, CO (40 bar), warmed up to 45°C, 20h, hydrolysis with H2SO4, sepn. of organic phase, dried, crystn. of organic products from hexane/CHCl3 = 20/1;
参考文献
Hoberg, Heinz; Fananas, F. Javier; Riegel, Hans Josef
Journal of Organometallic Chemistry, 1983 , vol. 254, # 2 p. 267 - 272
反应条件
(i) SO3, (ii) /BRN= 471175/, Et2O, cyclohexane; Multistep reaction;
参考文献
England,D.C. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 6181 - 6188
反应条件
di-tert-butyl peroxide
参考文献
Shono,T. et al.
Bulletin of the Chemical Society of Japan, 1964 , vol. 37, p. 635 - 637
参考文献
Milligan; Swan
Journal of the Chemical Society, 1959 , p. 2969,2976
参考文献
Walter,W.; Bode,K.-D.
Justus Liebigs Annalen der Chemie, 1962 , vol. 660, p. 74 - 84
参考文献
Lapkin,I.I.; Andreichikov,Yu.S.
Journal of Organic Chemistry USSR (English Translation), 1965 , vol. 1, p. 1223 - 1225
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, p. 1212 - 1214
参考文献
de Vries
Recueil des Travaux Chimiques des Pays-Bas, 1942 , vol. 61, p. 223,242, 243
Full Text Show Details
Grunfeld
Annales de Chimie (Cachan, France), 1933 , vol. <10> 20, p. 304,367
反应条件
Ambient temperature;
参考文献
Neidlein, Richard; Lehr, Werner
Heterocycles, 1981 , vol. 16, # 7 p. 1179 - 1185
反应条件
chromium other metals; Product distribution;
参考文献
Togashi, Shigeo; Fulcher, John G.; Cho, Bong Rae; Hasegawa, Minoru; Gladysz, J.A.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3044 - 3053