1: H2 / Pd/C / methanol / 18 h / 20 °C / 1500.15 Torr 2: triethylamine / methanol / 5 - 20 °C View Scheme
参考文献
Smith, Mark E.B.; Lloyd, Michael C.; Derrien, Nadine; Lloyd, Richard C.; Taylor, Stephen J.C.; Chaplin, David A.; Casy, Guy; McCague, Raymond
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 703 - 705
1.1: H2 / Pd/C / methanol / 18 h / 20 °C / 1500.15 Torr 2.1: triethylamine / methanol / 5 - 20 °C 3.1: triethylamine; DMAP / CH2Cl2 / 0.75 h / 0 °C 4.1: KOAc / dimethylformamide / 72 h / 60 °C 4.2: NaOMe / methanol / 7 h / 0 °C View Scheme
参考文献
Smith, Mark E.B.; Lloyd, Michael C.; Derrien, Nadine; Lloyd, Richard C.; Taylor, Stephen J.C.; Chaplin, David A.; Casy, Guy; McCague, Raymond
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 703 - 705
1: triethylamine / methanol / 16 h / 0 - 20 °C 2: H2 / [(S,S)-(Me-DuPHOS)-Rh(COD)]BF4 / methanol / 14 h / 20 °C / 3750.38 Torr View Scheme
参考文献
Smith, Mark E.B.; Lloyd, Michael C.; Derrien, Nadine; Lloyd, Richard C.; Taylor, Stephen J.C.; Chaplin, David A.; Casy, Guy; McCague, Raymond
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 703 - 705
1.1: triethylamine / methanol / 16 h / 0 - 20 °C 2.1: H2 / [(S,S)-(Me-DuPHOS)-Rh(COD)]BF4 / methanol / 14 h / 20 °C / 3750.38 Torr 3.1: triethylamine; DMAP / CH2Cl2 / 0.75 h / 0 °C 4.1: KOAc / dimethylformamide / 72 h / 60 °C 4.2: NaOMe / methanol / 7 h / 0 °C View Scheme
参考文献
Smith, Mark E.B.; Lloyd, Michael C.; Derrien, Nadine; Lloyd, Richard C.; Taylor, Stephen J.C.; Chaplin, David A.; Casy, Guy; McCague, Raymond
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 703 - 705
