9-甲基-9H-芴-9-羧酸合成路线 （共 23 条）
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane
T=30°C;
参考文献
Lindhardt, Anders T.; Simonssen, Roger; Taaning, Rolf H.; Gogsig, Thomas M.; Nilsson, Goeran N.; Stenhagen, Gunnar; Elmore, Charles S.; Skrydstrup, Troels
Journal of Labelled Compounds and Radiopharmaceuticals, 2012 , vol. 55, # 11 p. 411 - 418
反应条件
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 30 °C / Inert atmosphere
2: tri-tert-butyl phosphine; N-ethyl-N,N-diisopropylamine; m-xylene; bis(dibenzylideneacetone)-palladium(0) / 1,4-dioxane / 1.5 h / 80 °C / Inert atmosphere; Sealed vial
View Scheme
参考文献
AARHUS UNIVERSITET; SKRYDSTRUP, Troels; LINDHARDT, Anders Thyboe; HERMANGE, Philippe; TAANING, Rolf Hejle; FRIIS, Stig Duering
Patent: WO2012/79583 A1, 2012 ;
参考文献
Wislicenus; Mocker
Chemische Berichte, 1913 , vol. 46, p. 2790
