(2,2-二甲基-1,3-二氧戊环-4-基)甲基(9E)-9-十八碳烯酸酯合成路线 （共 17 条）
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide Esterification;
参考文献
Gras, Jean-Louis; Bonfanti, Jean-Francois
Synlett, 1999 , # 11 p. 1835 - 1837
参考文献
Journal of chemical ecology, , vol. 28, # 6 p. 1209 - 1220
反应条件
1: oct-7-enoic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester With 9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran 2: cis-1-iodo-1-decene With triphenyl-arsane; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=20°C; Suzuki coupling;
参考文献
Coleman, Bridgett E.; Cwynar, Valerie; Hart, David J.; Havas, Fabien; Jakkam, Madan Mohan; Patterson, Suzanne; Ridenour, Sam; Schmidt, Michael; Smith, Eboney; Wells, Angela J.
Synlett, 2004 , # 8 p. 1339 - 1342
反应条件
1.1: n-BuLi 1.2: I2 2.1: 55 percent / 2K(+)*(-)O2CN=NCO2(-); CH3CO2H / methanol 3.1: 9-BBN / tetrahydrofuran 3.2: 72 percent / aq. Cs2CO3; Ph3As / Pd(dppf)Cl2 / dimethylformamide / 20 °C View Scheme
参考文献
Synlett, , # 8 p. 1339 - 1342
反应条件
1.1: 72 percent / DCC; 4-DMAP / CH2Cl2 2.1: 9-BBN / tetrahydrofuran 2.2: 72 percent / aq. Cs2CO3; Ph3As / Pd(dppf)Cl2 / dimethylformamide / 20 °C View Scheme
参考文献
Synlett, , # 8 p. 1339 - 1342
反应条件
1.1: 55 percent / 2K(+)*(-)O2CN=NCO2(-); CH3CO2H / methanol 2.1: 9-BBN / tetrahydrofuran 2.2: 72 percent / aq. Cs2CO3; Ph3As / Pd(dppf)Cl2 / dimethylformamide / 20 °C View Scheme
参考文献
Synlett, , # 8 p. 1339 - 1342
反应条件
1.1: 72 percent / DCC; 4-DMAP / CH2Cl2 2.1: 9-BBN / tetrahydrofuran 2.2: 72 percent / aq. Cs2CO3; Ph3As / Pd(dppf)Cl2 / dimethylformamide / 20 °C View Scheme
参考文献
Synlett, , # 8 p. 1339 - 1342
反应条件
immobilized Rhizomucor miehei lipase in n-heptane T=60°C; 4 h; Enzymatic reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 77, p. 53 - 58
反应条件
sodium carbonate T=125 - 140°C; 6 h; Neat (no solvent);
参考文献
Journal of Thermal Analysis and Calorimetry, , vol. 106, # 3 p. 697 - 702
反应条件
1: aq. TFA / tetrahydrofuran / 0 °C 2: 55.2 percent / pyridine / 60 °C View Scheme
参考文献
Onodera, Junko; Matsuyama, Shigeru; Suzuki, Takahisa; Fujii, Koichi
Journal of chemical ecology, 2002 , vol. 28, # 6 p. 1209 - 1220
