1-(1,2-二甲基-1H-吲哚-3-基)乙酮合成路线 (共 8 条)
反应条件
trichlorophosphate in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl acetamide
参考文献
Wako Pure Chemical Industries, Ltd.
Patent: US5359085 A1, 1994 ;
参考文献
Watson, Darrell; Dillin, D. R.
Tetrahedron Letters, 1980 , vol. 21, p. 3969 - 3970
反应条件
BF4*Et2O 1.) ether, CH2Cl2, -13 deg C, 30 min, 2.) ether, CH2Cl2, RT, 30 min; Yield given. Multistep reaction;
参考文献
Janicki, Slawomir Z.; Schuster, Gary B.
Journal of the American Chemical Society, 1995 , vol. 117, # 33 p. 8524 - 8527
反应条件
12 h; Inert atmosphereReflux;
参考文献
Chen, Xi; Islamova, Nadezhda I.; Robles, Rachel V.; Lees, Watson J.
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 6 p. 1023 - 1029
参考文献
Chen, Yi; Zeng, De X.; Xie, Nan; Dang, Yi Z.
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5001 - 5005
反应条件
2: 35 percent / O2 / Irradiation View Scheme
参考文献
Watson, Darrell; Dillin, D. R.
Tetrahedron Letters, 1980 , vol. 21, p. 3969 - 3970
反应条件
2: 35 percent / O2 / Irradiation View Scheme
参考文献
Watson, Darrell; Dillin, D. R.
Tetrahedron Letters, 1980 , vol. 21, p. 3969 - 3970
反应条件
sodium hydroxide 1.) CH2Cl2, 2h, RT; Yield given. Multistep reaction;
参考文献
Pindur, Ulf; Flo, Camran; Akguen, Eyuep; Tunali, Mustafa
Liebigs Annalen der Chemie, 1986 , # 9 p. 1621 - 1627