(2E)-3-氯-1-苯基-2-丙烯-1-酮合成路线 (共 21 条)
反应条件
2: NH2OH*HCl / ethanol / 3 h / Heating
View Scheme
参考文献
Hauptmann,S.; Weisflog,J.
Journal fuer Praktische Chemie (Leipzig), 1972 , vol. 314, p. 353 - 364
反应条件
1: (i) Et3N, (ii) NaN3, H2O
2: NaOH
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参考文献
Nesmeyanov,A.N.; Rybinskaya,M.I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , p. 761 - 764
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , p. 816 - 820
反应条件
sodium in diethyl ether
参考文献
Belyaev,V.F.; Shamanovskaya,R.I.
Journal of Organic Chemistry USSR (English Translation), 1965 , vol. 1, p. 1405 - 1407
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, p. 1388 - 1390
参考文献
Cuvigny,T.; Normant,H.
Bulletin de la Societe Chimique de France, 1960 , p. 515 - 521
反应条件
sodium hydroxide
5 h; Heating;
参考文献
Baram. S. G.; Shkurko, O. P.; Mamaev, V. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 8 p. 1263 - 1267
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 8 p. 1781 - 1785
参考文献
Ritchie, Calvin D.; Kawasaki, Atsushi
Journal of Organic Chemistry, 1981 , vol. 46, # 23 p. 4704 - 4708
反应条件
1: benzene / Heating
2: aq. NaOH
View Scheme
参考文献
Zbiral,E.; Werner,E.
Justus Liebigs Annalen der Chemie, 1967 , vol. 707, p. 130 - 140
反应条件
potassium hydroxide; ethylene glycol
参考文献
Kotschetkow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 949,952; engl. Ausg. S. 977, 980
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2570,2573; engl. Ausg. S. 2533, 2535
反应条件
in N,N-dimethyl-formamide
参考文献
Shevelev,S.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1976 , vol. 25, # 12 p. 2535 - 2548
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1976 , vol. 25, # 12 p. 2725 - 2738
反应条件
bromine in tetrachloromethane
T=-10°C; 1 h;
参考文献
Kashima, Choji; Tajima, Tadakuni; Omote, Yoshimori
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 133 - 138