5-(4-甲氧基苯基)-1-苯基-1H-吡唑合成路线 (共 7 条)
反应条件
copper(l) iodide; triethylamine in acetonitrile T=82°C; 2 h; Inert atmosphere;
参考文献
Zora, Metin; Kivrak, Arif
Journal of Organic Chemistry, 2011 , vol. 76, # 22 p. 9379 - 9390
反应条件
N,N-dimethyl acetamide; (2',6'-dimethoxybiphenyl-2-yl)bis(4-(trifluoromethyl)phenyl)phosphine; palladium diacetate; potassium carbonate; silver carbonate; 2,2,2-trimethylacetic acid T=100°C; 16 h; Inert atmosphere;
参考文献
Rene, Olivier; Fagnou, Keith
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2116 - 2120
反应条件
in hydrogenchloride; methanol T=120°C; 0.0333333 h; microwave irradiation;
参考文献
Bagley, Mark C.; Lubinu, M. Caterina; Mason, Christopher
Synlett, 2007 , # 5 p. 704 - 708
反应条件
1: 65 percent / methanol / 5 h / Heating 2: 1N HCl / methanol / 1 h / Heating View Scheme
参考文献
Molina, P.; Fresneda, P. M.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 461 - 464
反应条件
1: 86 percent / dimethylformamide / 8 h / Heating 2: 65 percent / methanol / 5 h / Heating 3: 1N HCl / methanol / 1 h / Heating View Scheme
参考文献
Molina, P.; Fresneda, P. M.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 461 - 464
反应条件
1: boron trifluoride etherate / 1.) THF, reflux, 4 h; 2.) DMF, reflux, 5 h. 2: 86 percent / dimethylformamide / 8 h / Heating 3: 65 percent / methanol / 5 h / Heating 4: 1N HCl / methanol / 1 h / Heating View Scheme
参考文献
Molina, P.; Fresneda, P. M.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 461 - 464
反应条件
hydrogenchloride in methanol 1 h; Heating; Yield given. Yields of byproduct given;
参考文献
Molina, P.; Fresneda, P. M.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 461 - 464