反应条件
1: I2; NaHCO3 / ethanol 2: Lawesson's reagent / toluene / 0.5 h / Heating 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 6: ethanol / Heating 7: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 8: ethanol / Heating 9: I2; NaHCO3 / ethanol 10: Lawesson's reagent / toluene / 0.5 h / Heating 11: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 12: H2S / ethanol / pH 7.4 13: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 14: ethanol / Heating 15: I2; NaHCO3 / ethanol 16: Lawesson's reagent / toluene / 0.5 h / Heating 17: H2S / ethanol / pH 7.4 18: I2; NaHCO3 / ethanol 19: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 20: H2S / ethanol / pH 7.4 21: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 22: ethanol / Heating 23: I2; NaHCO3 / ethanol 24: Lawesson's reagent / toluene / 0.5 h / Heating 25: H2S / ethanol / pH 7.4 26: I2; NaHCO3 / ethanol 27: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 28: H2S / ethanol / pH 7.4 29: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 30: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 31: ethanol / Heating 32: P4S10 / xylene / 2 h / Heating 33: ethanol / Heating 34: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 35: I2; NaHCO3 / ethanol 36: Lawesson's reagent / toluene / 0.5 h / Heating 37: H2S / ethanol / pH 7.4 38: P4S10 / xylene / 2 h / Heating 39: ethanol / Heating 40: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
