2-氨基-6,7-二氢-5H-环戊[d]嘧啶-4-醇合成路线 （共 9 条）
反应条件
potassium carbonate in neat (no solvent) T=140°C; 0.166667 h; Microwave irradiation;
参考文献
Radhakrishnan; Sharma, Namita; Kundu, Lal Mohan
RSC Advances, 2014 , vol. 4, # 29 p. 15087 - 15090
反应条件
potassium tert-butylate in tert-butyl alcohol Reflux;
参考文献
Gangjee, Aleem; Zhao, Ying; Raghavan, Sudhir; Rohena, Cristina C.; Mooberry, Susan L.; Hamel, Ernest
Journal of Medicinal Chemistry, 2013 , vol. 56, # 17 p. 6829 - 6844
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
Full Text Show Details
Braker et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 3072,3075
Full Text Show Details
Biglino
Farmaco, Edizione Scientifica, 1957 , vol. 12, p. 72,75
反应条件
1: POCl3 2: ethanol; NH3 / 150 °C View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
反应条件
sulfuric acid; sodium nitrite
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
反应条件
1: POCl3 2: ethanol 3: Raney nickel; H2O View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
反应条件
1: POCl3
2: ethanol
3: water; methanol; NaOH
View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
反应条件
N,N-dimethyl-aniline; trichlorophosphate
T=135 - 140°C; 1 h;
参考文献
Ohno; Mizukoshi; Komatsu; Kunoh; Nakamura; Katoh; Nagasaka
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 10 p. 4150 - 4165
反应条件
1: POCl3
2: methanol; O,O'-dimethyl-diethylene glycol
View Scheme
参考文献
Ross et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3108,3111
