2-甲基-4-(4-硝基苯基)噻唑合成路线 (共 8 条)
反应条件
in ethylene glycol T=20°C; 0.0833333 h;
参考文献
Zhu, Dongjian; Chen, Jiuxi; Xiao, Huilong; Liu, Miaochang; Ding, Jinchang; Wu, Huayue
Synthetic Communications, 2009 , vol. 39, # 16 p. 2895 - 2906
反应条件
1: 4-nitrophenylacetoaldehyde With polymer-supported [(hydroxy(sulfonyloxy)iodo]benzene in acetonitrile 16 h; Heating; 2: ethanethioamide With potassium carbonate in acetonitrile 6 h; Heating;
参考文献
Ueno, Makoto; Togo, Hideo
Synthesis, 2004 , # 16 p. 2673 - 2677
反应条件
1: α-hydroxy-p-nitroacetophenone With triethylamine in dichloromethane 24 h; Heating; 2: ethanethioamide With potassium carbonate in acetonitrile 10 h; Heating; Further stages.;
参考文献
Liu, Xiao-Ling; Wang, Qiu-Ying; Sheng, Shou-Ri; Xu, Chen; Cai, Ming-Zhong
Synthetic Communications, 2008 , vol. 38, # 19 p. 3338 - 3345
参考文献
Ukrainskii Khimicheskii Zhurnal (Russian Edition), , vol. 25, p. 344,346
Chem.Abstr., , p. 5619
反应条件
1: 99 percent / iodosylbenzene / acetonitrile / 1.5 h / Heating 2: potassium carbonate / acetonitrile / 5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 16 p. 6424 - 6426
反应条件
1: AlCl3, aluminium chloride; bromine / chloroform / 45 °C 2: ethanol / 5 h / Reflux View Scheme
参考文献
Journal of Molecular Structure, , vol. 1000, # 1-3 p. 10 - 23
反应条件
potassium carbonate in acetonitrile 5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 16 p. 6424 - 6426
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate P=3000.3 Torr; 5 h;
参考文献
Dong Wha Pharm. Co., Ltd.
Patent: EP2394993 A2, 2011 ;
Location in patent: Page/Page column 18 ;