4-(2-丙炔氧基)苯甲腈合成路线 (共 5 条)
反应条件
potassium carbonate in 1-methyl-pyrrolidin-2-one T=85°C; 3 h;
参考文献
Okuno, Tsunehisa; Yamane, Kentaro; Sandman, Daniel J.
Molecular Crystals and Liquid Crystals, 2006 , vol. 456, # 1 p. 45 - 53
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tert.-butylhydroperoxide; potassium iodide in water T=20°C; 24 h;
参考文献
Lamani, Manjunath; Devadig, Pradeep; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 14 p. 2753 - 2759
反应条件
sodium azide; trifluorormethanesulfonic acid in acetonitrile T=20°C; Schmidt reaction; 0.0333333 h;
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5364 - 5370
反应条件
Cu(ClO4)2*6H2O; trimethylsilylazide; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,2-dichloro-ethane T=60°C; 2 h;
参考文献
Rokade, Balaji V.; Malekar, Sanjeev K.; Prabhu, Kandikere Ramaiah
Chemical Communications, 2012 , vol. 48, # 44 p. 5506 - 5508
反应条件
palladium on activated charcoal; ethanolamine in water T=80°C; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 54, # 9 p. 1169 - 1173