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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
33158-10-0
合成路线
（共 19 条）
18218-20-7
1-（1-（4-氯苯基）乙烯基）苯
→
反应条件
33158-10-0
反应条件
1: 72 percent / Mn(OAc)2, O2, AcOH / 23 °C 2: 32 percent / HClO4 / acetonitrile / 0.25 h / Heating View Scheme
参考文献
Qian, Chang-Yi; Hirose, Jun-ichi; Nishino, Hiroshi; Kurosawa, Kazu
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 5 p. 1219 - 1228
771477-46-4
→
反应条件
33158-10-0
反应条件
1: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 2: (Ph3P)AuCl; silver trifluoromethanesulfonate / dichloromethane / 0.08 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
33948-36-6
1-(4-喹啉基)甲胺
→
反应条件
33158-10-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.67 h / 0 °C / |Inert atmosphere 2: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 3: (Ph3P)AuCl; silver trifluoromethanesulfonate / dichloromethane / 0.08 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
536-74-3
苯乙炔
→
反应条件
33158-10-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.67 h / 0 °C / |Inert atmosphere 2: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 3: (Ph3P)AuCl; silver trifluoromethanesulfonate / dichloromethane / 0.08 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
203519-47-5
→
反应条件
33158-10-0
反应条件
1: 82 percent / NaBH4 / methanol / 25 °C 2: NaN3 / dimethylformamide / 3 h / 60 °C View Scheme
参考文献
Dartiguelongue; Seraphin; Duval; Gomes
Pharmacy and Pharmacology Communications, 1998 , vol. 4, # 1 p. 13 - 16
70-11-1
→
反应条件
33158-10-0
反应条件
1: KOH 2: H2SO4 View Scheme
参考文献
Stetter; Siehnhold
Chemische Berichte, 1955 , vol. 88, p. 271,274
771477-46-4
→
反应条件
1839-72-1
+
33158-10-0
反应条件
1: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 2: silver trifluoromethanesulfonate; methanol; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl; toluene-4-sulfonic acid / dichloromethane-d2 / 0.17 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
33948-36-6
1-(4-喹啉基)甲胺
→
反应条件
1839-72-1
+
33158-10-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.67 h / 0 °C / |Inert atmosphere 2: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 3: silver trifluoromethanesulfonate; methanol; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl; toluene-4-sulfonic acid / dichloromethane-d2 / 0.17 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
536-74-3
苯乙炔
→
反应条件
1839-72-1
+
33158-10-0
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.67 h / 0 °C / |Inert atmosphere 2: tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide / dichloromethane; water / 0 °C 3: silver trifluoromethanesulfonate; methanol; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl; toluene-4-sulfonic acid / dichloromethane-d2 / 0.17 h / 20 °C View Scheme
参考文献
Wang, Tao; Shi, Shuai; Vilhelmsen, Mie Hojer; Zhang, Tuo; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Chemistry - A European Journal, 2013 , vol. 19, # 37 p. 12512 - 12516
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