Boc-4-叠氮-Phe-OH合成路线 (共 3 条)
反应条件
imidazole-1-sulfonyl azide hydrochloride; triethylamine; zinc(II) chloride in methanol; acetonitrile T=20°C; 12 h; DarknessInert atmosphere;
参考文献
Strom, T. Amanda; Barron, Andrew R.
Chemical Communications, 2010 , vol. 46, # 26 p. 4764 - 4766
反应条件
copper(l) iodide; sodium azide; L-proline; sodium hydroxide in dimethyl sulfoxide
参考文献
Zhu, Wei; Ma, Dawei
Chemical communications (Cambridge, England), 2004 , # 7 p. 888 - 889
反应条件
1: tetrahydrofuran / 1 h / 20 °C 2: H2O / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 25 p. 4467 - 4470