2-(4-溴苯基)丙烯酸乙酯合成路线 (共 3 条)
反应条件
potassium carbonate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=60°C; 2 h;
参考文献
Liang, Chungen; Tang, Guozhi; Wong, Jason Christopher; Wu, Xihan
Patent: US2010/69328 A1, 2010 ;
Location in patent: Page/Page column 31 ;
反应条件
1: α-bromoacrylate d'ethyle With naphthalene; N(Et)4ClO4; zinc in N,N-dimethyl-formamide T=-20°C; 1 h; 2: 4-bromo-1-iodobenzene With bis (triortho-tolylphosphine)palladium(II) chloride in N,N-dimethyl-formamide T=70°C; 3 h;
参考文献
Jalil, Aishah A; Kurono, Nobuhito; Tokuda, Masao
Tetrahedron, 2002 , vol. 58, # 37 p. 7477 - 7484
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride; zinc in tetrahydrofuran; N,N-dimethyl-formamide 3 h; Heating;
参考文献
Jalil, Aishah A; Kurono, Nobuhito; Tokuda, Masao
Tetrahedron, 2002 , vol. 58, # 37 p. 7477 - 7484