4-甲氧基-α-甲基苯甲醇合成路线 （共 290 条）
反应条件
hydrogen; Ru(1,3-dimesityl-2,3-dihydro-1H-imidazol-2-yl)(PPh3)2CO(H)2 in benzene T=70°C; P=3800 Torr; 24 h;
参考文献
Castro, Luis C. Misal; Bezier, David; Sortais, Jean-Baptiste; Darcel, Christophe
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1279 - 1284
反应条件
formic acid; C29H32ClIrNO; sodium formate in water T=80°C; pH=4.8; 0.25 h; Inert atmosphereSealed tube; Reagent/catalyst;
参考文献
WO2013/153407 A1, ;
Paragraph 00163; 00168 ;
反应条件
sodium tetrahydroborate; Fe pythalocyanine; oxygen in ethanol T=0 - 25°C; P=760.051 Torr; 3 h; Inert atmosphere;
参考文献
Leggans, Erick K.; Barker, Timothy J.; Duncan, Katharine K.; Boger, Dale L.
Organic Letters, 2012 , vol. 14, # 6 p. 1428 - 1431
反应条件
Novozym 435; 2,6-dimethylheptan-4-ol; (Ph4C4CO)2H(μ-H)(CO)4Ru2 in toluene T=70°C; Reduction; 42 h; Enzymatic reaction;
参考文献
Organic Letters, , vol. 2, # 3 p. 409 - 411
反应条件
naphthalene; lithium; manganese (II) chloride in tetrahydrofuran T=28 - 30°C; 1 h; sonication;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 8 p. 1720 - 1723
反应条件
sodium hydroxide; RuCl2(PPh3)(iBu-BTP) T=82°C; P=750.075 Torr; 6 h;
参考文献
Yu; Zeng; Sun; Deng; Dong; Chen; Wang; Pei
Journal of Organometallic Chemistry, 2007 , vol. 692, # 11 p. 2306 - 2313
反应条件
1: With 1-bromo-butane; sodium tetrahydroborate; Aliquatreg; 336 T=20°C; Addition; Hydroboration; 16 h; 2: With sodium hydroxide; dihydrogen peroxide T=40°C; Oxidation; 1 h;
参考文献
Synlett, , # 7 p. 997 - 998
反应条件
1: methyl iodide With magnesium in tetrahydrofuran 1 h; Heating; 2: 4-methoxy-benzaldehyde in tetrahydrofuran T=20°C; 3 h;
参考文献
Sharma, Gangavaram V. M.; Reddy, Katta Laxmi; Lakshmi, P. Sree; Ravi; Kunwar, Ajit C.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3967 - 3969
反应条件
in diethyl ether T=0 - 5°C; Grignard reaction; 2 h;
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
反应条件
potassium tert-butylate; (η5-C5Ph5)Ru(CO)2Cl in isopropyl alcohol; toluene T=20°C; 1.25 h;
参考文献
Tetrahedron Letters, , vol. 45, # 36 p. 6799 - 6802
