4-甲氧基-α-甲基苯甲醇合成路线 (共 290 条)
反应条件
N-oxyl-immobilized silica gel; sodium hydrogencarbonate; sodium bromide in water; acetone Electrolysissolid phase reaction;
参考文献
Synthesis, , # 6 art. no. F20808SS, p. 903 - 908
反应条件
Et3N-WS-TEMPO bromide in water T=0°C; Electrochemical reaction;
参考文献
Tetrahedron Letters, , vol. 46, # 52 p. 8975 - 8979
反应条件
PE-N-oxyl; sodium hydrogencarbonate; sodium bromide T=5°C; Electrolysis;
参考文献
Synlett, , # 7 p. 951 - 954
反应条件
Tris-HCl buffer T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
反应条件
ammonia; iodine in water T=60°C; Lieben-Haller-Bauer reaction; 2 h;
参考文献
Cao, Liping; Ding, Jiaoyang; Gao, Meng; Wang, Zihua; Li, Juan; Wu, Anxin
Organic Letters, 2009 , vol. 11, # 17 p. 3810 - 3813
反应条件
hydroxylamine hydrochloride; trichlorophosphate 1.) 30 min, 55-65 deg C; 1 h, 75-85 deg C, 2.) 125 deg C; Yield given. Multistep reaction;
参考文献
Liebscher, Juergen; Bechstein, Ute
Zeitschrift fuer Chemie (Stuttgart, Germany), 1984 , vol. 24, # 2 p. 56 - 57
反应条件
C15H17N2Ru(1+)*F6P(1-); sodium t-butanolate in toluene T=110°C; 17 h; Inert atmosphere;
参考文献
Chang, Xu; Chuan, Low Wei; Yongxin, Li; Pullarkat, Sumod A.
Tetrahedron Letters, 2012 , vol. 53, # 12 p. 1450 - 1455
反应条件
lipase B from Candida antarctica in toluene T=78°C; 48 h; Enzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
反应条件
tris-(dibenzylideneacetone)dipalladium(0); CsOH; 2,6-bis(N-butyl-N'-methylenebenzimidazolium)-1-bromophenylene dibromide; hydrogen in para-xylene T=125°C; P=760.051 Torr;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 4 p. 896 - 900
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; potassium hydroxide in 1,4-dioxane T=80°C; 40 h;
参考文献
Applied Organometallic Chemistry, , vol. 25, # 9 p. 695 - 698