4-甲氧基-α-甲基苯甲醇合成路线 （共 290 条）
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; dodec-1-ene; potassium hydroxide in 1,4-dioxane T=80°C; 40 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
thiophene; Sodium tetrachloroaurate(III) in dichloromethane 9 h; Reflux;
参考文献
Ohshima, Takashi; Nakahara, Yasuhito; Ipposhi, Junji; Miyamoto, Yoshiki; Mashima, Kazushi
Chemical Communications, 2011 , vol. 47, # 29 p. 8322 - 8324
反应条件
lipase B from Candida antarctica in toluene T=78°C; 48 h; Enzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
反应条件
potassium hydroxide; dodec-1-ene; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane T=80°C; 20 h;
参考文献
Cho, Chan Sik; Kim, Bok Tae; Choi, Heung-Jin; Kim, Tae-Jeong; Shim, Sang Chul
Tetrahedron, 2003 , vol. 59, # 40 p. 7997 - 8002
反应条件
thionyl chloride in dichloromethane T=-78°C; 0.25 h; Inert atmosphere;
参考文献
Waibel, Michael; Kieser, Karen J.; Carlson, Kathryn E.; Stossi, Fabio; Katzenellenbogen, Benita S.; Katzenellenbogen, John A.
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 9 p. 3560 - 3570
反应条件
1: 65 percent / phosphoryl chloride / 3 h / Heating 2: sodium hydride / 1,2-dimethoxy-ethane 3: 6.7 g / KOH / methanol / 6 h / Heating View Scheme
参考文献
Koul, Surrinder; Koul, Jawahir L.; Taneja, Subhash C.; Dhar, Kanaya L.; Jamwal, Deshvir S.; Singh, Kuldeep; Reen, Rashmeet K.; Singh, Jaswant
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 251 - 268
反应条件
1: H3[PW12O40] / dimethyl sulfoxide / 1 h / 100 °C / Inert atmosphere 2: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triethylamine; [(t-Bu)3PH]BF4 / N,N-dimethyl-formamide / 4 h / 100 °C View Scheme
参考文献
Colbon, Paul; Barnard, Jonathan H.; Purdie, Mark; Mulholland, Keith; Kozhevnikov, Ivan; Xiao, Jianliang
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1395 - 1400
反应条件
1: 4-methoxy-α-methylbenzyl alcohol With [Pd(η3-allyl)(Cl)((N,N′-bis-(2,6-diisopropylphenyl)imidazol-2-ylidene))]; 4-methyl-chlorobenzene; potassium tert-butylate in toluene T=40°C; 3 h; Inert atmosphere; 2: chlorobenzene in toluene T=80°C; 4 h; Inert atmosphere;
参考文献
Landers, Brant; Berini, Christophe; Wang, Chao; Navarro, Oscar
Journal of Organic Chemistry, 2011 , vol. 76, # 5 p. 1390 - 1397
反应条件
tricarbonyl(tetraphenylcyclopentadienone)iron; N,N,N-triethylamine N-oxide in acetone T=60°C; 24 h; Inert atmosphere;
参考文献
Johnson, Tarn C.; Clarkson, Guy J.; Wills, Martin
Organometallics, 2011 , vol. 30, # 7 p. 1859 - 1868
反应条件
lipase B from Candida antarctica in toluene T=78°C; 48 h; Enzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
