4-甲氧基-α-甲基苯甲醇合成路线 (共 290 条)
反应条件
N-(quinolin-2-ylmethylidene)aniline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in acetone T=30°C; 5 h; Inert atmosphereSchlenk technique;
参考文献
Tetrahedron, , vol. 69, # 8 p. 2033 - 2037
反应条件
1-butyl-2-isopropyl-3-methylimidazolium triflimide in tetrahydrofuran T=20°C; 2 h;
参考文献
Handy, Scott T.
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4659 - 4662
反应条件
sodium hydroxide; sodium tetrahydroborate; oxygen; 5,10,15,20-tetrakis(1-methyl-4-pyridino)porphyrine tertachloride in water Ambient temperaturepH 12;
参考文献
Chemistry Letters, , # 3 p. 519 - 522
反应条件
chloro-trimethyl-silane; tetrakis(dimethylamino)ethylene; Chromium (III) chloride; niobium bromide in N,N-dimethyl-formamide T=20°C; Acylation; Reduction; 6 h;
参考文献
Synlett, , # 12 p. 1930 - 1932
反应条件
1: dimethyl zinc; phenylacetylene in dichloromethane T=0°C; 0.5 h; 2: With titanium(IV) isopropylate; C22H21F6NO7S in dichloromethane T=0°C; 1.5 h; 3: 4-methoxy-benzaldehyde optical yield given as percent eeenantioselective reactionFurther stages;
参考文献
Tetrahedron Letters, , vol. 52, # 38 p. 4882 - 4884
反应条件
1: With [RuN(saldach)(CH3OH)](+)[ClO4](-); phenyl silane in toluene 13 h; Reflux; 2: With hydrogenchloride in diethyl ether; water; toluene
参考文献
ACS Catalysis, , vol. 3, # 4 p. 678 - 684
反应条件
sodium hydroxide in water T=0°C; 14 h; Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 1009 - 1027
反应条件
bis(acetylacetonate)nickel(II); triphenylphosphine in tetrahydrofuran; hexane T=0°C; 0.5 h;
参考文献
Ichiyanagi, Tsuyoshi; Kuniyama, Satoru; Shimizu, Makoto; Fujisawa, Tamotsu
Chemistry Letters, 1998 , # 10 p. 1033 - 1034
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol T=20°C; 17 h;
参考文献
Angewandte Chemie - International Edition, , vol. 48, # 3 p. 539 - 542
反应条件
diphosphorous tetraiodide; tetraethylammonium bromide; water in dichloromethane T=20°C; 6 h; regioselective reaction;
参考文献
Telvekar, Vikas N.; Rane, Rajesh A.
Synthetic Communications, 2010 , vol. 40, # 14 p. 2108 - 2112