4-甲氧基-α-甲基苯甲醇合成路线 (共 290 条)
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; [bis(triphenyl-λ5-phosphanylidene)ammonium][Cl]; acetone; potassium hydroxide; N,N'-bis[o-(diphenylphosphino)benzylidene]-(1S,2S)-diaiminocyclohexane in dichloromethane; water; isopropyl alcohol T=28°C; 5.5 h; Resolution of racemateInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Zhang, Juanni; Yang, Xiangren; Zhou, Han; Li, Yanyun; Dong, Zhenrong; Gao, Jingxing
Green Chemistry, 2012 , vol. 14, # 5 p. 1289 - 1292
反应条件
N,N,N-triethylamine N-oxide; C14H16FeO5Si in toluene T=60°C; 6 h; Inert atmosphere;
参考文献
Johnson, Tarn C.; Clarkson, Guy J.; Wills, Martin
Organometallics, 2011 , vol. 30, # 7 p. 1859 - 1868
反应条件
tricarbonyl(tetraphenylcyclopentadienone)iron; N,N,N-triethylamine N-oxide in acetone T=60°C; 24 h; Inert atmosphere;
参考文献
Johnson, Tarn C.; Clarkson, Guy J.; Wills, Martin
Organometallics, 2011 , vol. 30, # 7 p. 1859 - 1868
反应条件
in acetone T=25°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 35, # 47 p. 8751 - 8754
反应条件
lt;Mn3O(OAc)6(OAc)(HOAc)gt;*5H2O; lithium chloride in acetic acid 0.2 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 11 p. 3567 - 3571
反应条件
air; [NMQ][BF4] in dichloromethane 0.5 h; UV-irradiation; Product distributionQuantum yield; Further Variations:ReagentsSolvents;
参考文献
Physical Chemistry Chemical Physics, , vol. 10, # 1 p. 200 - 210
反应条件
NbCl5 in acetonitrile
T=20°C; 0.333333 h;
参考文献
Srihari, Pabbaraja; Bhunia, Dinesh C.; Sreedhar, Pamu; Yadav, Jhillu S.
Synlett, 2008 , # 7 p. 1045 - 1049
反应条件
[Fe(III)(TPP)]SbF6 in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts Alkylation; 5 h; Sealed tubeInert atmosphere; Overall yield = 73 percent; regioselective reaction;
参考文献
Teranishi, Satoru; Kurahashi, Takuya; Matsubara, Seijiro
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-U0620-L, p. 2148 - 2152
反应条件
H3[PW12O40] in methoxybenzene
T=130°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Colbon, Paul; Barnard, Jonathan H.; Purdie, Mark; Mulholland, Keith; Kozhevnikov, Ivan; Xiao, Jianliang
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1395 - 1400
反应条件
palladium dichloro (η-2,5-norbornadiene); oxygen; (-)-sparteine in toluene
T=80°C; 96 h;
参考文献
Ferreira; Stoltz
Journal of the American Chemical Society, 2001 , vol. 123, # 31 p. 7725 - 7726