4-甲氧基-α-甲基苯甲醇合成路线 (共 290 条)
反应条件
Candida antarctica lipase B; (η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene
T=20°C; 6 h;
参考文献
Martin-Matute, Belen; Edin, Michaela; Bogar, Krisztian; Kaynak, F. Betuel; Baeckvall, Jan-E.
Journal of the American Chemical Society, 2005 , vol. 127, # 24 p. 8817 - 8825
反应条件
Escherichia coli BioH in hexane
T=35°C; 28 h; Resolution of racemate; enantioselective reaction;
参考文献
Wang, Bo; Tang, Xiaoling; Liu, Ji; Yu, Hongwei
Tetrahedron Letters, 2010 , vol. 51, # 48 p. 6360 - 6364
参考文献
Nakamura, Kaoru; Inoue, Yuko; Matsuda, Tomoko; Misawa, Ibuki
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2397 - 2402
反应条件
immobilized green pea protein; Pisum sativum L in water
T=35°C; Oxidation; optical resolution; 192 h; Title compound not separated from byproducts;
参考文献
Nagaoka; Kayahara
Bioscience, biotechnology, and biochemistry, 2000 , vol. 64, # 4 p. 781 - 784
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene
T=70°C; P=142.511 Torr; 40 h;
参考文献
Verzijl, Gerard K.M.; De Vries, Johannes G.; Broxterman, Quirinus B.
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1603 - 1610
反应条件
immobilized Candida antarctica Lipase B; potassium carbonate; 1-(4-methoxyphenyl)ethanone; chiral ruthenium-based in toluene
T=70°C; P=150.012 Torr; 31 h;
参考文献
van Nispen, Sjoerd F.G.M.; van Buijtenen, Jeroen; Vekemans, Jef A.J.M.; Meuldijk, Jan; Hulshof, Lumbertus A.
Tetrahedron Asymmetry, 2006 , vol. 17, # 15 p. 2299 - 2305
反应条件
RuCl(η5-C9H7)(PPh3)2; Pseudomonas cepocia lipase; triethylamine
T=60°C; Esterification; resolution of racemate; 43 h; Enzymatic reaction;
参考文献
Koh, Jeong Hwan; Jung, Hyun Min; Kim, Mahn-Joo; Park, Jaiwook
Tetrahedron Letters, 1999 , vol. 40, # 34 p. 6281 - 6284
反应条件
potassium phosphate; Novozym 435; (CO)2ClRu(benzyloxytetraphenylpentadienyl) in toluene
T=25°C; 30 h;
参考文献
Kim, Namdu; Ko, Soo-Byung; Min, Serk Kwon; Kim, Mahn-Joo; Park, Jaiwook
Organic Letters, 2005 , vol. 7, # 20 p. 4523 - 4526
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene
T=40°C; 4 h;
参考文献
Bouzemi, Nassima; Aribi-Zouioueche, Louisa; Fiaud, Jean-Claude
Tetrahedron Asymmetry, 2006 , vol. 17, # 5 p. 797 - 800
反应条件
1,3-bis-[(R)-1-(1-naphthyl)ethyl]-4,5-dihydro-3H-imidazolium tetrafluoroborate; potassium tert-butylate in tetrahydrofuran
T=-78 - -40°C; 5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Kano, Taichi; Sasaki, Kouji; Maruoka, Keiji
Organic Letters, 2005 , vol. 7, # 7 p. 1347 - 1349