4-甲氧基-α-甲基苯甲醇合成路线 （共 290 条）
反应条件
Tris-HCl buffer
T=30°C; pH=7.5; 24 h; Enzymatic reaction; enantioselective reaction;
参考文献
Bisogno, Fabricio R.; Lavandera, Ivan; Kroutil, Wolfgang; Gotor, Vicente
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1730 - 1732
反应条件
Candida antarctica lipase immobilized on magnetic nanoparticles in tert-butyl methyl ether
T=32°C; 24 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Netto, Caterina G.C.M.; Andrade, Leandro H.; Toma, Henrique E.
Tetrahedron Asymmetry, 2009 , vol. 20, # 19 p. 2299 - 2304
反应条件
lipase YS in di-isopropyl ether
T=30°C; 29 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Naemura, Koichiro; Fukuda, Ritsuko; Konishi, Masayoshi; Hirose, Keiji; Tobe, Yoshito
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1253 - 1256
反应条件
lipase B from Candida antarctica in toluene
T=78°C; 48 h; Enzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
反应条件
lipase B from Candida antarctica in toluene
T=70°C; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
反应条件
Candida antarctica lipase B in tert-butyl methyl ether
16 h; Enzymatic reaction; optical yield given as percent ee;
参考文献
Brossat, Maude; Moody, Thomas S.; Nanteuil, Florian De; Taylor, Stephen J.C.; Vaughan, Fatima
Organic Process Research and Development, 2009 , vol. 13, # 4 p. 706 - 709
反应条件
1: With Candida antarctica lipase B in tert-butyl methyl ether
16 h; Enzymatic reaction;
2: With hydrogenchloride; water in methanol
optical yield given as percent ee;
参考文献
Brossat, Maude; Moody, Thomas S.; Nanteuil, Florian De; Taylor, Stephen J.C.; Vaughan, Fatima
Organic Process Research and Development, 2009 , vol. 13, # 4 p. 706 - 709
反应条件
60 h; Ambient temperaturedifferent time, other tertiary amine S-(-)-N,N-dimethyl-α-(p-nitrophenyl)ethylamine (III); Product distribution;
参考文献
Potapov, V. M.; Dem'yanovich, V. M.; Khlebnikov, V. A.; Koval'skaya, S. S.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 8 p. 1602 - 1606
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 8 p. 1753 - 1758
参考文献
The United States of America as represented by the Secretary of Agriculture
Patent: US4342777 A1, 1982 ;
反应条件
in acetic-formic acid
参考文献
The United States of America as represented by the Secretary of Agriculture
Patent: US4342777 A1, 1982 ;
