4-甲氧基-α-甲基苯甲醇合成路线 （共 290 条）
反应条件
1: With copper(l) chloride in various solvent(s) T=20°C; Reduction; Coupling; Silylation; 24 h; 2: With water; toluene-4-sulfonic acid in various solvent(s) T=20°C; Hydrolysis;
参考文献
Synlett, , # 4 p. 479 - 482
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; [(1,3-(2,6-iPr2C6H3)2-1,3-dihydroimidazol-2-ylidene)PdCl2]2 in 1,2-dichloro-ethane T=65°C; 20 h; Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 5, # 1 p. 63 - 65
反应条件
benzo[1,3,2]dioxaborole; 1,3-dibutyl-4,5-dichloro-imidazole-1,3-divinylsiloxane Pt(0) in tetrahydrofuran T=25°C; 3 h;
参考文献
Chemical Communications, , # 21 p. 2184 - 2186
反应条件
1: With formic acid T=100°C; 5 h; Inert atmosphereSealed tube; 2: With chloro-(pentamethylcyclopentadienyl)-{5-methoxy-2-{1-[(4-methoxyphenyl)imino-N]ethyl}phenyl-C}-iridium(lll); water; sodium formate T=20 - 80°C; pH=3.5; 6 h;
参考文献
Li, Jia; Wang, Chao; Xue, Dong; Wei, Yawen; Xiao, Jianliang
Green Chemistry, 2013 , vol. 15, # 10 p. 2685 - 2689
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran T=20°C; Decomposition;
参考文献
Journal of Organic Chemistry, , vol. 65, # 9 p. 2834 - 2836
反应条件
1: 1-bromo-butane With magnesium; ethylene dibromide in 2-methyl tetrahydrofuran T=20°C; Inert atmosphere; 2: 1-(4-methoxyphenyl)ethanone in 2-methyl tetrahydrofuran T=0 - 20°C; Grignard reaction; 1.25 h; Inert atmosphere; chemoselective reaction;
参考文献
Journal of Chemical Research, , # 6 p. 370 - 373
反应条件
titanium(IV) isopropylate; zinc(II) chloride in toluene T=-78 - -30°C;
参考文献
Omote, Masaaki; Tanaka, Naoya; Tarui, Atsushi; Sato, Kazuyuki; Kumadaki, Itsumaro; Ando, Akira
Tetrahedron Letters, 2007 , vol. 48, # 17 p. 2989 - 2991
反应条件
sodium in 1-methyl-pyrrolidin-2-one 0.5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 67, # 6 p. 1776 - 1780
反应条件
naphthalene; lithium in tetrahydrofuran T=-78 - 0°C; 2 h;
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1996 , vol. 52, # 45 p. 14341 - 14348
反应条件
in tetrahydrofuran T=-78°C; 0.166667 h;
参考文献
Gimisis, Thanasis; Arsenyan, Pavel; Georganakis, Dimitris; Leondiadis, Leondios
Synlett, 2003 , # 10 p. 1451 - 1454
