2-甲基-4-硫氰酰基苯胺合成路线 （共 10 条）
反应条件
silica boron sulfonic acid; dihydrogen peroxide in water 0.75 h; regioselective reaction;
参考文献
Khazaei, Ardeshir; Zolfigol, Mohammad Ali; Safaiee, Maliheh; Mokhlesi, Mohammad; Donyadari, Elmira; Shiri, Morteza; Kruger, Hendrik Gerhardus
Catalysis Communications, 2012 , vol. 26, p. 34 - 38
反应条件
bromo-dimethylsulfonium bromide in acetonitrile T=20°C; 0.25 h;
参考文献
Bhalerao, Dinesh S.; Akamanchi, Krishnacharya G.
Synlett, 2007 , # 19 p. 2952 - 2956
反应条件
Mn(OAc)3 in acetic acid T=25°C; 2 h; regioselective reaction;
参考文献
Pan, Xiang-Qiang; Lei, Mao-Yi; Zou, Jian-Ping; Zhang, Wei
Tetrahedron Letters, 2009 , vol. 50, # 3 p. 347 - 349
参考文献
Horii
Yakugaku Zasshi, 1935 , vol. 55, p. 14,20;dtsch.Ref.S.4
Chem.Abstr., 1935 , p. 3317
参考文献
Helwig
Patent: US1816848 , 1929 ;
Full Text Show Details
Melnikow; Sskljarenko; Tscherkassowa
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 1819,1821
Chem. Zentralbl., 1940 , vol. 111, # I p. 1641
参考文献
Helwig
Patent: US1816848 , 1929 ;
Full Text Show Details
Melnikow; Sskljarenko; Tscherkassowa
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 1819,1821
Chem. Zentralbl., 1940 , vol. 111, # I p. 1641
反应条件
ammonium hydroxide in 1,4-dioxane
T=100°C; sealed ampoule;
参考文献
Rybin, A. G.; Zil'berman, E. N.; Zhivoderov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1863 - 1867,1677 - 1680
反应条件
1: 89 percent / dioxane
2: 90.5 percent / 23percent aq. ammonia / dioxane / 100 °C / sealed ampoule
View Scheme
参考文献
Rybin, A. G.; Zil'berman, E. N.; Zhivoderov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1863 - 1867,1677 - 1680
参考文献
Rybin, A. G.; Zil'berman, E. N.; Zhivoderov, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1863 - 1867,1677 - 1680
参考文献
Lichoscherstow; Petrow
Zhurnal Obshchei Khimii, 1933 , vol. 3, p. 759,761,763
Chem. Zentralbl., 1934 , vol. 105, # II p. 3620
Full Text Show Details
Takatori
Yakugaku Zasshi, 1947 , vol. 67, p. 191
Chem.Abstr., 1951 , p. 9497
