2,2,2-三氟-4’-甲氧基乙酰苯胺合成路线 （共 11 条）
反应条件
sodium hydride in N,N-dimethyl-formamide T=20°C;
参考文献
Mekhalfia, Abdelaziz; Mutter, Roger; Heal, William; Chen, Beining
Tetrahedron, 2006 , vol. 62, # 24 p. 5617 - 5625
反应条件
triethylamine; trichloroacetonitrile; triphenylphosphine in acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
Han, Ki-Jong; Kim, Misoo
Letters in Organic Chemistry, 2011 , vol. 8, # 8 p. 559 - 561
反应条件
potassium carbonate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane T=75°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in N,N-dimethyl-formamide T=45°C;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
lanthanum trifluoromethanesulphonate T=20°C; 1 h; Inert atmosphere; chemoselective reaction;
参考文献
Morimoto, Hiroyuki; Fujiwara, Risa; Shimizu, Yuhei; Morisaki, Kazuhiro; Ohshima, Takashi
Organic Letters, 2014 , vol. 16, # 7 p. 2018 - 2021
反应条件
in anhydrous xylene 6.5 h; Reflux;
参考文献
Ohtaka, Junpei; Sakamoto, Takeshi; Kikugawa, Yasuo
Tetrahedron Letters, 2009 , vol. 50, # 15 p. 1681 - 1683
反应条件
chloro-trimethyl-silane 1 h; Heating;
参考文献
Barua, Apurba; Bez, Ghanashyam; Barua, Nabin C.
Synlett, 1999 , # 5 p. 553 - 554
反应条件
benzenesulphinic acid sodium salt in N,N-dimethyl-formamide
参考文献
Tetrahedron Letters, , vol. 43, # 40 p. 7189 - 7191
反应条件
1: 27 percent / NaH / tetrahydrofuran / 24 h / 20 °C 2: 90 percent / NaBH4 / tetrahydrofuran / 12 h View Scheme
参考文献
Brigas, Amadeu F.; Clegg, William; Dillon, Christopher J.; Fonseca, Custodia F.C.; Johnstone, Robert A.W.
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 8 p. 1315 - 1324
反应条件
sodium hydroxide; potassium carbonate in acetonitrile T=25°C; 1.5 h;
参考文献
Albanese; Penso
Synthesis, 1991 , # 11 p. 1001 - 1002
